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[姜黄油超临界CO₂流体萃取的工艺研究]

[Technological study on the supercritical-CO2 fluid extraction of Curcuma longa oils].

作者信息

Ge F, Shi Q, Tan X, Li Z, Jing X

机构信息

Guangzhou Pharmaceutical Industrial Research Institute, Guangzhou 510240.

出版信息

Zhong Yao Cai. 1997 Jul;20(7):345-50.

Abstract

This paper first reports technological study on the extraction of Curcuma longa oils by supercritical-CO2 fluid, mainly studies the influence of pressure, temperature, flow rate of CO2 and time on the yield of the oils, determines optimum technology of extracting the oils, analyzes chemical constituents extracted, compares the oils from SFE-CO2 and SD technology, studies industrial test on the SF-CO2 extraction. The results shows pressure and temperature are more important factors of influence; the optimum technological condition is the extracted pressure 25 MPa and temperature 45 degrees C, isolated pressure I 12.5 MPa and temperature I 60 degrees C, isolated pressure II 6MPa and temperature II 38 degrees C, CO2 flow rate 9 Kg/Kg.h, and extracted time 2 h; the constituents from SFE-CO2 and SD methods are identical, but their content has some difference; SFE-CO2 technology is better than that of SD, which is high yield shorter time, etc.; the industrial production of the oils with SFE-CO2 method is available.

摘要

本文首次报道了超临界CO₂流体萃取姜黄油的工艺研究,主要研究了压力、温度、CO₂流速和时间对姜黄油得率的影响,确定了姜黄油的最佳萃取工艺,分析了萃取出的化学成分,比较了超临界CO₂萃取法(SFE-CO₂)和水蒸气蒸馏法(SD)所得的姜黄油,研究了SFE-CO₂萃取的工业化试验。结果表明,压力和温度是更重要的影响因素;最佳工艺条件为萃取压力25MPa、温度45℃,分离压力Ⅰ12.5MPa、温度Ⅰ60℃,分离压力Ⅱ6MPa、温度Ⅱ38℃,CO₂流速9kg/(kg·h),萃取时间2h;SFE-CO₂法和SD法所得成分相同,但含量有差异;SFE-CO₂工艺优于SD法,具有得率高、时间短等优点;采用SFE-CO₂法进行姜黄油的工业化生产是可行的。

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