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冷原子荧光法测定甘草中的痕量汞

[Determination of trace mercury in the liquorice by cold atomic fluorometry].

作者信息

Shi J, Li J, Qu L

机构信息

School of Chemistry and Chemical Engineering, Zhengzhou University, 450052 Zhengzhou.

出版信息

Guang Pu Xue Yu Guang Pu Fen Xi. 2001 Aug;21(4):558-9.

Abstract

By applying the nondispersive apparatus with reduction and gasification, and the wet dissolving method, the trace mercury in liquorice is determined by cold atomic fluorometry. We studied the conditions that can affect the determined results. We compared two methods for cleaning the glass ware, and contrasted the working curve method with addition plotting method. We also studied the applicability of this experimental method. The recovery is 86.9%-110.8%, and the error is less than 13.1%. It proves the method is efficient and satisfactory.

摘要

采用还原气化非分散装置及湿法溶解,用冷原子荧光法测定甘草中的微量汞。研究了影响测定结果的条件,比较了两种玻璃器皿清洗方法,对比了工作曲线法和标准加入法,研究了该实验方法的适用性。回收率为86.9% - 110.8%,相对误差小于13.1%,证明该方法高效且令人满意。

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