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[高温拉曼光谱技术的发展]

[Developments of high temperature Raman spectroscopic techniques].

作者信息

Jiang G, You J, Yu B, Haung S

机构信息

Shanghai Enhanced Laboratory of Ferrometallurgy, Shaghai University, 200072 Shanghai.

出版信息

Guang Pu Xue Yu Guang Pu Fen Xi. 2000 Apr;20(2):206-9, 221.

Abstract

High temperature Raman spectroscopy (HTRS) is contemporarily a useful tool to study micro-structure of various materials under high temperature. Developments of HTRS techniques are well reviewed. In order to realize the determinations of metallurgical melts, the modified instrumentation for high temperature determination purpose based on JY U1000 Raman spectrometer in Shanghai Enhanced Lab of Ferrometallurgy (SELF) is introduced. It is assembled as macro-Raman with time-resolved detect system by using pulsed Copper Vapor Laser(CVL). This is the first set of its kind in domestic and some further modifications are proposed.

摘要

高温拉曼光谱(HTRS)是目前研究各种材料在高温下微观结构的一种有用工具。HTRS技术的发展已有详尽综述。为实现对冶金熔体的测定,介绍了上海铁冶金强化实验室(SELF)基于JY U1000拉曼光谱仪改装的用于高温测定的仪器。它通过使用脉冲铜蒸气激光器(CVL)组装成具有时间分辨检测系统的宏观拉曼光谱仪。这是国内首套此类仪器,并提出了一些进一步的改进建议。

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