Xu F, Xiao Z S, Cheng G A, Yi Z Z, Zeng Y X, Zhang T H, Gu L L
Surface Physics Laboratory, Fudan University, Shanghai 200433, China.
Guang Pu Xue Yu Guang Pu Fen Xi. 2001 Dec;21(6):758-62.
Er ions with 108 keV to a dose of 1 x 10(17) cm-2 were implanted into Si-rich thermal oxidation SiO2/Si thin film using metal vapor vacuum arc (MEVVA) ion source implanter. Er concentration in as-implanted sample, which was attained to -10 at % correspond to the level of -10(21) atoms.cm-3, was analyzed by Rutherford back-scattering (RBS) and X-ray photoelectron spectroscope (XPS). Contents of Er, Si and O in annealed samples were investigated using XPS at room temperature. It showed that Si content was increased and SiO2 content was decreased with increasing the fluence of Si ions. It was found by use dof reflective high energy electron diffraction (RHEED) and atomic force microscope (AFM) that needle micro-crystalline Si in the surface of annealed samples had been formed and Er segregation and precipitation were formed little. Photoluminescence around 1.54 microns from Er-doped Si-rich thermal oxidized SiO2/Si thin film were studied with a He-Cd laser pumping at 414.6 nm at the low temperature of 77 K and room-temperature (RT).
使用金属蒸汽真空弧(MEVVA)离子源注入机,将能量为108 keV、剂量为1×10¹⁷ cm⁻² 的铒离子注入富硅热氧化SiO₂/Si薄膜中。通过卢瑟福背散射(RBS)和X射线光电子能谱仪(XPS)分析了注入态样品中的铒浓度,其达到-10原子百分比,对应于-10²¹ 原子·cm⁻³ 的水平。在室温下使用XPS研究了退火样品中铒、硅和氧的含量。结果表明,随着硅离子注量的增加,硅含量增加而SiO₂ 含量降低。通过反射高能电子衍射(RHEED)和原子力显微镜(AFM)发现,退火样品表面形成了针状微晶硅,铒的偏析和沉淀很少。在77 K低温和室温(RT)下,用414.6 nm的氦镉激光泵浦,研究了掺铒富硅热氧化SiO₂/Si薄膜在1.54微米附近的光致发光。