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[肉豆蔻的薄层色谱鉴别及其引入日本非药典生药标准]

[Identification of nutmeg by thin-layer chromatography and its introduction to Japanese standards for non-pharmacopoeial crude drugs].

作者信息

Suzuki H, Harada M

出版信息

Eisei Shikenjo Hokoku. 1990(108):98-100.

PMID:1364369
Abstract

When nutmeg was extracted with hot methanol and cooled, much precipitate was produced. The colorless crystals, obtained on recrystallization, were identified as trimyristin by spectroscopic means and by direct comparison with the standard. Then, the identification of nutmeg was established by using the same extraction as above and subjecting the precipitate to thin-layer chromatography. This method was newly introduced to the Standards for Non-pharmacopoeial Crude Drugs.

摘要

肉豆蔻用热甲醇萃取并冷却后,产生了大量沉淀。通过重结晶得到的无色晶体,经光谱分析并与标准品直接比较,鉴定为肉豆蔻酸甘油三酯。然后,采用上述相同的萃取方法,对沉淀进行薄层色谱分析,从而确立了肉豆蔻的鉴别方法。该方法新被引入《非药用天然药物标准》。

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