[采用离子对高效液相色谱法测定含大黄的东方药剂汤液中的番泻苷A]
[Determination of sennoside A in oriental pharmaceutical decoctions containing Rhei Rhizoma by ion-pair high-performance liquid chromatography].
作者信息
Momma N, Ueda J, Ohsawa K
机构信息
Tohoku College of Pharmacy, Sendai, Japan.
出版信息
Yakugaku Zasshi. 1992 Apr;112(4):272-5. doi: 10.1248/yakushi1947.112.4_272.
PMID:1403660
Abstract
A simple method using ion-pair high-performance liquid chromatography was established for the rapid and precise determination of sennoside A in oriental pharmaceutical decoctions containing Rhei Rhizoma. This method was compared with other two methods, i.e. ion-suppression and phosphate buffer methods. Sennoside A was eluted without interference in this ion-pair method, while the determination of sennoside A was interfered by co-existing components in the other two methods.
摘要
建立了一种采用离子对高效液相色谱法快速、准确测定含大黄的中药汤剂中番泻苷A的简便方法。该方法与另外两种方法，即离子抑制法和磷酸盐缓冲液法进行了比较。在这种离子对方法中，番泻苷A的洗脱不受干扰，而在另外两种方法中，番泻苷A的测定受到共存成分的干扰。
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引用本文的文献
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Simple and rapid analysis of sennoside A and sennoside B contained in crude drugs and crude drug products by solid-phase extraction and high-performance liquid chromatography.通过固相萃取和高效液相色谱法对生药及生药制品中含有的番泻苷A和番泻苷B进行简单快速分析。
J Nat Med. 2010 Apr;64(2):126-32. doi: 10.1007/s11418-009-0377-x. Epub 2009 Dec 17.
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