压力对微波增强的狄尔斯-阿尔德反应的影响。一项案例研究。
The effect of pressure on microwave-enhanced Diels-Alder reactions. A case study.
作者信息
Kaval Nadya, Dehaen Wim, Kappe C Oliver, Van der Eycken Erik
机构信息
Department of Chemistry, Katholieke Universiteit Leuven, Leuven, Belgium.
出版信息
Org Biomol Chem. 2004 Jan 21;2(2):154-6. doi: 10.1039/b315150f. Epub 2003 Dec 4.
DOI:10.1039/b315150f
PMID:14737635
Abstract
It is demonstrated that microwave-assisted Diels-Alder reactions of substituted 2(1H)-pyrazinones with ethylene are significantly more effective utilizing pre-pressurized (up to 10 bar) reaction vessels.
摘要
结果表明，在使用预加压（高达10巴）反应容器时，取代的2(1H)-吡嗪酮与乙烯的微波辅助狄尔斯-阿尔德反应显著更有效。
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