Sergeeva Tatiana A, Dolbier William R
Department of Chemistry, University of Florida, Gainesville, Florida 32611, USA.
Org Lett. 2004 Jul 8;6(14):2417-9. doi: 10.1021/ol0491991.
[reaction: see text] A new and convenient three-step synthesis of pentafluorosulfanylbenzene from 1,4-cyclohexadiene with an overall yield of >70% is reported along with a number of derivatization reactions.
[反应:见正文] 报道了一种以1,4-环己二烯为原料,全新且便捷的三步合成五氟硫烷基苯的方法,总产率>70%,同时还包括一些衍生化反应。