Cullum Hazel E, McGavigan Claire, Uttley Claire Z, Stroud Mark A M, Warren Derek C
Forensic Explosives Laboratory, Defence Science and Technology Laboratory, Fort Halstead, Sevenoaks, Kent, UK.
J Forensic Sci. 2004 Jul;49(4):684-90.
This survey was carried out as a follow-up to a 1994 survey carried out by this laboratory (1) in order to determine the background levels of explosives traces in public places. The first survey concentrated on transport areas and police stations in and around London. This second study examines levels in four of the United Kingdom's major cities: Birmingham, Cardiff, Glasgow, and Manchester. Samples were taken at various transport sites and from hotels, private houses, private vehicles, and clothing. The survey showed that traces of the high explosives nitroglycerine (NG), trinitrotoluene (TNT), pentaerythritol tetranitrate (PETN), and cyclotrimethylene trinitramine (RDX) are rare within the general public environment. Only one low-level trace of RDX was detected. NG, possibly associated with the use of firearms, was detected at low levels in two samples and 2,4-DNT was detected in a separate sample. No PETN was detected in any of the samples. The results of the survey indicate that it is unlikely that persons visiting public areas could become significantly contaminated with explosives. The analytical procedures employed would also have detected ethylene glycol dinitrate (EGDN) if present at levels greater than 2 ng, nitrobenzene (NB) if present at levels greater than 50 ng, mononitrotoluenes if present at levels greater than 50 ng, and the other common isomers of dinitrotoluene if these had been present at levels in excess of 10 ng. None of these were detected. The relatively high volatility of EGDN, NB, and the mononitrotoluenes would, however, cause traces of these compounds to disperse rapidly. A proportion of the samples (approximately 7%) were analyzed for the presence of HMX. No HMX was detected.
本次调查是作为本实验室于1994年开展的一项调查(1)的后续行动进行的,目的是确定公共场所爆炸物痕迹的背景水平。第一次调查集中在伦敦及其周边的交通区域和警察局。第二项研究考察了英国四个主要城市(伯明翰、加的夫、格拉斯哥和曼彻斯特)的水平。在不同的交通站点以及酒店、私人住宅、私人车辆和衣物上采集了样本。调查显示,在一般公共环境中,高爆炸物硝化甘油(NG)、三硝基甲苯(TNT)、季戊四醇四硝酸酯(PETN)和环三亚甲基三硝胺(RDX)的痕迹很少见。仅检测到一处低水平的RDX痕迹。在两个样本中检测到了可能与枪支使用有关的低水平NG,在另一个单独样本中检测到了2,4 -二硝基甲苯(2,4 - DNT)。在任何样本中均未检测到PETN。调查结果表明,前往公共场所的人员不太可能受到爆炸物的显著污染。如果乙二醇二硝酸酯(EGDN)的含量高于2纳克、硝基苯(NB)的含量高于50纳克、一硝基甲苯的含量高于50纳克以及二硝基甲苯的其他常见异构体的含量超过10纳克,所采用的分析程序也能够检测到它们。但这些物质均未被检测到。然而,EGDN、NB和一硝基甲苯相对较高的挥发性会导致这些化合物的痕迹迅速扩散。对一部分样本(约7%)分析了奥克托今(HMX)的存在情况。未检测到HMX。