Petersen R C
University of Alabama at Birmingham, School of Engineering, Department of Biomedical Engineering, Hoehn Building, Room 330, Birmingham, AL 35294, USA.
J Dent Res. 2005 Apr;84(4):365-70. doi: 10.1177/154405910508400414.
Micromechanical physics of critical fiber length, describing a minimum filament distance for resin impregnation and stress transfer, has not yet been applied in dental science. As a test of the hypothesis that 9-micron-diameter, 3-mm-long quartz fibers would increase mechanical strength over particulate-filled composites, photocure-resin-pre-impregnated discontinuous reinforcement was incorporated at 35 wt% into 3M Corporation Z100, Kerr Corporation HerculiteXRV, and an experimental photocure paste with increased radiopaque particulate. Fully articulated four-point bend testing per ASTM C 1161-94 for advanced ceramics and Izod impact testing according to a modified unnotched ASTM D 256-00 specification were then performed. All photocure-fiber-reinforced composites demonstrated significant improvements over particulate-filled compounds (p < 0.001) for flexural strength, modulus, work of fracture, strain at maximum load, and Izod toughness, with one exception for the moduli of Z100 and the experimental reinforced paste. The results indicate that inclusion of pre-impregnated fibers above the critical aspect ratio yields major advancements regarding the mechanical properties tested.
描述树脂浸渍和应力传递所需最小长丝间距的临界纤维长度微机械物理学,尚未应用于牙科科学。作为对直径9微米、长3毫米的石英纤维比颗粒填充复合材料机械强度更高这一假设的测试,将光固化树脂预浸渍的不连续增强材料以35 wt% 的比例掺入3M公司的Z100、 Kerr公司的HerculiteXRV以及一种含更多不透射线颗粒的实验性光固化糊剂中。然后按照针对高级陶瓷的ASTM C 1161-94进行全铰接四点弯曲测试,并根据修改后的无缺口ASTM D 256-00规范进行悬臂梁冲击测试。所有光固化纤维增强复合材料在弯曲强度、模量、断裂功、最大载荷下的应变和悬臂梁韧性方面均比颗粒填充复合材料有显著改善(p < 0.001),Z100和实验性增强糊剂的模量除外。结果表明,包含高于临界长径比的预浸渍纤维会在测试的机械性能方面带来重大进展。