Petersen Richard C, Wenski Edward G
R&D Faculty, Inc., Biomaterials Group, Kansas City, Missouri, 64112.
Mechanical and Thermal Analysis Analytical Laboratory, United States Department of Energy Federal Manufacturing and Technologies, Operated by Honeywell International, Kansas City, Missouri 64141.
Int SAMPE Symp Exhib. 2002 May;47:380-394.
The objective was to validate strength improvements by incorporating chopped fiber into commercial particulate filled visible-light cured dental pastes. Photocurable resin preimpregnated 3-mm high purity quartz fibers were blended into two universal commercial composites, 3M Corp. Z100 and Kerr Corp. XRV at 35 wt% fiber. Four groups, consisting of the Z100 and XRV controls, along with Z100 and XRV both containing fibers, were prepared in a mold 2×2×25-mm then cured at equivalent irradiation intensities monitored by a Demetron Radiometer. Evaluation was accomplished on ten specimens from the four different categories according to ASTM Standard C 1161-94 configuration-A utilizing a fully-articulated four-point bend fixture and 20-mm span. Five samples out of each group were further assessed using a modified Izod Plastic Impact Tester per ASTM D 256-00. Both highly strengthened fiber reinforced composites attained a marginal error of uncertainty for statistical significance over the commercial controls (p=0.001 AVOVA posthoc Newman-Keuls) with maximum bending stress, flexural modulus, work of fracture and Izod impact toughness. From the results, it can be concluded that photocured chopped fiber reinforced composites will produce improvements over particulate filled compounds that can be considered breakthrough.
目的是通过将短切纤维加入商用颗粒填充可见光固化牙科糊剂中来验证强度的提高。将光固化树脂预浸渍的3毫米高纯度石英纤维以35重量%的纤维比例混入两种通用商用复合材料中,即3M公司的Z100和 Kerr公司的XRV。制备四组样本,包括Z100和XRV对照组,以及都含有纤维的Z100和XRV组,在一个2×2×25毫米的模具中成型,然后在由Demetron辐射计监测的等效辐照强度下固化。根据ASTM标准C 1161 - 94配置A,使用全铰接四点弯曲夹具和20毫米跨度,对来自四个不同类别的十个样本进行评估。每组中的五个样本进一步按照ASTM D 256 - 00,使用改进的悬臂梁式塑料冲击试验机进行评估。两种高强度纤维增强复合材料在最大弯曲应力、弯曲模量、断裂功和悬臂梁冲击韧性方面,相对于商用对照材料均达到了具有统计学显著性的微小误差(p = 0.001,方差分析后纽曼 - 基尔斯检验)。从结果可以得出结论,光固化短切纤维增强复合材料相对于颗粒填充化合物将产生改进,这可被视为突破性进展。