Fleming Garry J P, Nolan Lawrence, Harris Jonathan J
Biomaterials Unit, School of Dentistry, University of Birmingham, St Chad's Queensway, Birmingham B4 6NN, UK.
J Dent. 2005 May;33(5):405-12. doi: 10.1016/j.jdent.2004.10.025. Epub 2004 Dec 20.
To assess the effect of interfacial surface roughness on the flexure strength and fracture mode and origin utilizing an in-vitro assessment of the clinical failure conditions expected for all-ceramic crowns and the connector area of fixed partial dentures (FPDs) using bilayered ceramic specimens tested in bi-axial flexure.
Sets of 20 bilayered composite discs, with core:dentine thickness ratio of 2:1 and interfacial surface roughnesses determined by alumina abrasion with different alumina particle sizes, were tested in bi-axial flexure with both the reinforcing core and veneering dentine loaded in tension. Mean flexure strengths, standard deviations and associated Weibull Moduli (m) were determined. Optical microscopy was employed for identification of the fracture mode and origin for the failure all-ceramic crowns and the connector area of FPDs.
The interfacial surface roughness influenced the bi-axial flexure strength and reliability of the flexure strength data when both the reinforcing core and veneering dentine porcelain were tested in tension. The number of fracture fragments, frequency of occurrence of specimen delaminations, Hertzian cone formations and sub-critical radial cracking in the bilayered dental ceramic composite disc-shaped specimens was also dependent on the interfacial surface roughness and the surface loaded in tension.
The fracture resistance, failure mode and failure origin in bilayered ceramics tested to represent the clinical failure mode of all-ceramic crowns and FPDs are dependent upon the interfacial surface roughness and the modulus of the material in tension.
通过对双层陶瓷试件进行双轴弯曲测试,模拟全瓷冠和固定局部义齿(FPD)连接体区域预期的临床失效情况,体外评估界面粗糙度对弯曲强度、断裂模式及起源的影响。
制备20组双层复合圆盘,其核层与牙本质层厚度比为2:1,通过使用不同粒径氧化铝进行研磨来确定界面粗糙度,对增强核层和饰面牙本质层均施加拉伸载荷,进行双轴弯曲测试。测定平均弯曲强度、标准差及相关韦布尔模量(m)。采用光学显微镜识别全瓷冠和FPD连接体区域失效的断裂模式及起源。
当增强核层和饰面牙本质瓷均承受拉伸载荷时,界面粗糙度影响双轴弯曲强度及弯曲强度数据的可靠性。双层牙科陶瓷复合圆盘形试件中的断裂碎片数量、试件分层的发生频率、赫兹圆锥形成及亚临界径向裂纹也取决于界面粗糙度和承受拉伸载荷的表面。
模拟全瓷冠和FPD临床失效模式测试的双层陶瓷的抗断裂性、失效模式及失效起源取决于界面粗糙度和承受拉伸载荷材料的模量。