Monticelli Francesca, Toledano Manuel, Tay Franklin R, Cury Alvaro H, Goracci Cecilia, Ferrari Marco
Department of Restorative Dentistry and Dental Materials, University of Siena, Policlinico Le Scotte, Viale Bracci, 53100 Siena, Italy.
Dent Mater. 2006 Jul;22(7):602-9. doi: 10.1016/j.dental.2005.05.018. Epub 2005 Nov 14.
To verify the influence of different etching procedures of the post-surface on microtensile bond strength values between fiber posts and composite core materials.
60 DT Light Posts were divided into 10 subgroups using five different chemical surface treatments and two composite materials to build-up the abutment. Chemical surface treatments including etching with potassium permanganate; treatment with 10% hydrogen peroxide; treatment with 21% sodium ethoxide; etching with potassium permanganate and 10 vol.% HCl; silanization (control group) were performed on the post's surface. The build-up was performed using (A) Core Paste XP (Dent Mat) and (B) Unifil Flow (GC). Two samples of each group were randomly selected to investigate the morphologic aspect of the post/core interface with a scanning electron microscope (SEM). The remaining specimens were cut so as to obtain microtensile sticks that were loaded in tension at a cross-head speed of 1mm/min until failure. The statistical analysis was performed using two-way ANOVA and the Tukey's test for post-hoc comparisons (alpha=0.05).
SEM examination showed an interpenetrating adhesion network between the treated fiber post-surface and the composite material in all the groups tested. The results achieved with potassium permanganate had a significant influence on microtensile interfacial bond strength values with both the tested materials. Post-superficial treatments enhanced the bond strength particularly of Core Paste XP.
Etching procedures showed a similar effect on the post-surface and enhanced the adhesion of composite core build-ups as a result of micromechanical and chemical retention.
验证桩表面不同蚀刻程序对纤维桩与复合树脂核材料之间微拉伸粘结强度值的影响。
将60根DT Light桩分为10个亚组,采用五种不同的化学表面处理方法和两种复合材料制作基台。化学表面处理包括用高锰酸钾蚀刻;用10%过氧化氢处理;用21%乙醇钠处理;用高锰酸钾和10 vol.%盐酸蚀刻;硅烷化处理(对照组)。使用(A)Core Paste XP(Dent Mat)和(B)Unifil Flow(GC)进行堆塑。每组随机选取两个样本,用扫描电子显微镜(SEM)观察桩/核界面的形态。将其余标本切割成微拉伸试件,以1mm/min的十字头速度进行拉伸加载直至破坏。采用双向方差分析和Tukey事后检验进行统计学分析(α = 0.05)。
SEM检查显示,在所有测试组中,处理后的纤维桩表面与复合材料之间存在互穿粘结网络。高锰酸钾处理的结果对两种测试材料的微拉伸界面粘结强度值有显著影响。桩表面处理增强了粘结强度,尤其是对Core Paste XP。
蚀刻程序对桩表面有类似的影响,并通过微机械和化学固位作用增强了复合树脂核堆塑的粘结力。