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施加电压对电泳沉积法制备的钛基羟基磷灰石涂层的影响。

Effects of applied voltages on hydroxyapatite coating of titanium by electrophoretic deposition.

作者信息

Meng Xianwei, Kwon Tae-Yub, Yang Yunzhi, Ong Joo L, Kim Kyo-Han

机构信息

Institute for Biomaterials Research & Development, Kyungpook National University, Daegu, South Korea.

出版信息

J Biomed Mater Res B Appl Biomater. 2006 Aug;78(2):373-7. doi: 10.1002/jbm.b.30497.


DOI:10.1002/jbm.b.30497
PMID:16362967
Abstract

Hydroxyapatite (HA) coatings were deposited on titanium substrates by electrophoretic deposition (EPD) at constant voltage and dynamic voltage, respectively. Various surface morphologies were observed under different type of voltages. Under a constant voltage of 20 V, a dense HA coating could be prepared. Under a constant voltage of 200 V, big HA particles were deposited and the coating was porous. Under a dynamic voltage, a continuous gradient HA coating could be obtained. HA coatings were characterized with a field emission-scanning electron microscopy (FE-SEM) and an X-ray diffraction (XRD). XRD indicated no significant HA decomposition when the coatings were sintered for 2 h at 800 degrees C.

摘要

分别通过在恒定电压和动态电压下的电泳沉积(EPD),将羟基磷灰石(HA)涂层沉积在钛基底上。在不同类型的电压下观察到了各种表面形态。在20V的恒定电压下,可以制备出致密的HA涂层。在200V的恒定电压下,沉积了大的HA颗粒,涂层是多孔的。在动态电压下,可以获得连续的梯度HA涂层。通过场发射扫描电子显微镜(FE-SEM)和X射线衍射(XRD)对HA涂层进行了表征。XRD表明,当涂层在800℃下烧结2小时时,HA没有明显分解。

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