Cox M, Klass G
Forensic Science South Australia, 21 Divett Place, Adelaide, SA, Australia.
Forensic Sci Int. 2006 Dec 20;164(2-3):138-47. doi: 10.1016/j.forsciint.2005.12.019. Epub 2006 Jan 25.
This paper reports the identification of a number of by-products, which are produced during the Wacker oxidation of safrole to 3,4-methylenedioxyphenyl-2-propanone (MDP2P) using rho-benzoquinone and palladium chloride when methanol is utilised as the solvent. Also described is the retrieval of these compounds from illicit samples from a clandestine laboratory, which was uncovered in South Australia in September 2003.
本文报道了一些副产物的鉴定结果，这些副产物是在以甲醇为溶剂，利用对苯醌和氯化钯将黄樟素瓦克氧化为3,4-亚甲基二氧苯基-2-丙酮（MDP2P）的过程中产生的。文中还描述了从一个于2003年9月在南澳大利亚发现的秘密实验室的非法样品中获取这些化合物的情况。
