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牙科陶瓷中断裂韧性与抗弯强度之间的关系。

Relationship between fracture toughness and flexural strength in dental porcelains.

作者信息

Cesar Paulo Francisco, Yoshimura Humberto Naoyuki, Miranda Walter Gomes, Miyazaki Caroline Lumi, Muta Luciana Mayumi, Rodrigues Filho Leondardo Eloy

机构信息

Department of Dental Materials, School of Dentistry, University of São Paulo, São Paulo, Brazil.

出版信息

J Biomed Mater Res B Appl Biomater. 2006 Aug;78(2):265-73. doi: 10.1002/jbm.b.30482.

Abstract

The aim of this study was to investigate the correlation between fracture toughness (K(Ic)) and flexural strength (FS) in dental porcelains. Porcelains with different leucite contents and clinical indications were used (A, B, C, D, and E). K(Ic) was determined by surface crack in flexure method (SCF) and FS was determined by four-point-bending test. Microstructural characterization was also carried out. The leucite contents of porcelains A, B, C, D, and E were, respectively, 22, 22, 6, 15, and 0%. Materials with higher leucite content (A and B) presented significantly higher K(Ic) values compared to materials with lower leucite content (C and E). The Weibull moduli (m) of porcelains A and B were statistically higher than those of the other three materials. Regarding characteristic strength (sigma(0)), porcelains D and E showed similar values and statistically higher than those of the other materials which were statistically different from each other. According to the regression analysis, sigma(0) increased with the increase of K(Ic) until approximately 0.75 MPa m(1/2). After that, the increase in K(Ic) was accompanied by a decrease in sigma(0). However, the Weibull modulus increased with the increase in K(Ic), especially for values greater than 0.80 MPa m(1/2).

摘要

本研究的目的是调查牙科陶瓷的断裂韧性(K(Ic))与弯曲强度(FS)之间的相关性。使用了具有不同白榴石含量和临床适应症的陶瓷(A、B、C、D和E)。通过弯曲表面裂纹法(SCF)测定K(Ic),通过四点弯曲试验测定FS。还进行了微观结构表征。陶瓷A、B、C、D和E的白榴石含量分别为22%、22%、6%、15%和0%。与白榴石含量较低的材料(C和E)相比,白榴石含量较高的材料(A和B)的K(Ic)值显著更高。陶瓷A和B的威布尔模量(m)在统计学上高于其他三种材料。关于特征强度(sigma(0)),陶瓷D和E显示出相似的值,并且在统计学上高于其他材料,而其他材料之间在统计学上彼此不同。根据回归分析,sigma(0)随着K(Ic)的增加而增加,直到大约0.75 MPa m(1/2)。在那之后,K(Ic)的增加伴随着sigma(0)的降低。然而,威布尔模量随着K(Ic)的增加而增加,特别是对于大于0.80 MPa m(1/2)的值。

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