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Complete assignments of the 1H and 13C NMR spectra of 9,10-didehydro retinoic acids.

作者信息

Thibonnet J, Duchêne A, Parrain J-L, Abarbri M

机构信息

Laboratoire de Synthèse et Physicochimie Organique et Thérapeutique, Faculté des Sciences de Tours, Parc de Grandmont, EA 3857, 37200 Tours, France.

出版信息

Magn Reson Chem. 2006 Jun;44(6):651-3. doi: 10.1002/mrc.1800.

Abstract

A new class of retinoic acids was synthesized containing a 9,10-rigid bond. 1H and 13C NMR spectra were assigned for eight new compounds (all-E, 13Z) containing a carboxylic acid or tertiobutylester polar end group. Assignments were based on the combination of one- and two-dimensional experiments (APT, COSY, HMBC).

摘要

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Complete assignments of the 1H and 13C NMR spectra of 9,10-didehydro retinoic acids.
Magn Reson Chem. 2006 Jun;44(6):651-3. doi: 10.1002/mrc.1800.

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