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5-取代-4-（亚芳基）氨基-2,4-二氢-3H-1,2,4-三唑-3-硫酮和6-芳基-3-（D-葡萄糖戊糖醇-1-基）-7H-1,2,4-三唑并[3,4-b][1,3,4]噻二嗪的1H和13C核磁共振研究

1H and 13C NMR study of 5-substituted-4- (arylidene)amino-2,4-dihydro-3H-1,2,4-triazole-3-thiones and 6-aryl-3-(D-gluco- pentitol-1-yl)-7H-1,2,4-triazolo[3,4-b] [1,3,4]thiadiazines.

作者信息

Zhang Anjiang, Zhang Lixue, Lei Xinxiang

机构信息

Department of Chemistry, Wenzhou University, Wenzhou 325035, China.

出版信息

Magn Reson Chem. 2006 Aug;44(8):813-6. doi: 10.1002/mrc.1829.

DOI:10.1002/mrc.1829
PMID:16625670
Abstract

Five 5-substituted-4-(arylidene)amino-2,4-dihydro-3H-1, 2,4-triazole-3-thiones (2a-2e) and seven 6-aryl-3-(D-gluco-pentitol-1-yl)-7H-1,2,4-triazolo[3,4-b][1,3,4]thiadiazines (3a-3g) were synthesized. The complete 1H and 13C NMR chemical shift assignments were analyzed on one- and two-dimensional NMR techniques, including DEPT, NOE-DIF, COSY, gHMBC, and gHSQC.

摘要

合成了5个5-取代-4-（亚芳基）氨基-2,4-二氢-3H-1,2,4-三唑-3-硫酮（2a - 2e）和7个6-芳基-3-（D-葡萄糖戊糖醇-1-基）-7H-1,2,4-三唑并[3,4-b][1,3,4]噻二嗪（3a - 3g）。利用包括DEPT、NOE-DIF、COSY、gHMBC和gHSQC在内的一维和二维核磁共振技术对其完整的1H和13C核磁共振化学位移归属进行了分析。

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