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牛关节软骨硫酸角质素中α(1-3)连接岩藻糖残基质子共振的完整归属

A full assignment of proton resonances for an alpha(1-3)-linked fucose residue in keratan sulphate from bovine articular cartilage.

作者信息

Huckerby T N, Nieduszynski I A, Brown G M, Cockin G H

机构信息

Department of Chemistry, Lancaster University, Bailrigg, UK.

出版信息

Glycoconj J. 1991 Feb;8(1):39-44. doi: 10.1007/BF00731641.

DOI:10.1007/BF00731641
PMID:1668530
Abstract

Full proton NMR assignments have been achieved for the alpha(1-3)-linked fucose residues contained in alkaline borohydride reduced keratan sulphate chains derived from bovine articular cartilage. This involved 500 MHz spectroscopy at 60 degrees C and included COSY and RELAYED-COSY determinations.

摘要

已完成对源自牛关节软骨的碱性硼氢化物还原硫酸角质素链中含有的α(1-3)连接岩藻糖残基的全质子核磁共振归属。这涉及在60℃下的500兆赫光谱分析，包括同核去偶相关谱（COSY）和接力同核去偶相关谱（RELYED-COSY）测定。

相似文献

1
A full assignment of proton resonances for an alpha(1-3)-linked fucose residue in keratan sulphate from bovine articular cartilage.牛关节软骨硫酸角质素中α(1-3)连接岩藻糖残基质子共振的完整归属
Glycoconj J. 1991 Feb;8(1):39-44. doi: 10.1007/BF00731641.
2
Fucose content of keratan sulphates from bovine articular cartilage.来自牛关节软骨的硫酸角质素的岩藻糖含量。
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3
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4
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Biochem J. 1998 Mar 1;330 ( Pt 2)(Pt 2):753-7. doi: 10.1042/bj3300753.
3
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VARIATIONS IN KERATOSULFATES.硫酸角质素的变异
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Mucopolysaccharides of costal cartilage.肋软骨的黏多糖
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A non-reducing terminal fragment from tracheal cartilage keratan sulphate chains contains alpha (2-3)-linked N-acetylneuraminic acid.来自气管软骨硫酸角质素链的一个非还原性末端片段含有α(2-3)连接的N-乙酰神经氨酸。
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Degradation of articular cartilage keratan sulphates using hydrazinolysis and nitrous acid. Environment of fucose residues.利用肼解和亚硝酸降解关节软骨硫酸角质素。岩藻糖残基的环境。
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Primary-structure determination of fourteen neutral oligosaccharides derived from bronchial-mucus glycoproteins of patients suffering from cystic fibrosis, employing 500-MHz 1H-NMR spectroscopy.利用500兆赫的1H核磁共振光谱法对来自囊性纤维化患者支气管黏液糖蛋白的14种中性寡糖进行一级结构测定。
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Primary structure determination of five sialylated oligosaccharides derived from bronchial mucus glycoproteins of patients suffering from cystic fibrosis. The occurrence of the NeuAc alpha(2----3)Gal beta(1----4)[Fuc alpha(1----3)] GlcNAc beta(1----.) structural element revealed by 500-MHz 1H NMR spectroscopy.源自囊性纤维化患者支气管黏液糖蛋白的五种唾液酸化寡糖的一级结构测定。通过500兆赫1H核磁共振光谱揭示的NeuAcα(2→3)Galβ(1→4)[Fucα(1→3)]GlcNAcβ(1→.)结构元件的存在情况。
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Stage-specific embryonic antigen involves alpha 1 goes to 3 fucosylated type 2 blood group chains.阶段特异性胚胎抗原涉及α1至3岩藻糖基化的2型血型链。
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Studies on keratosulfates. Methylation, desulfation, and acid hydrolysis studies on old human rib cartilage keratosulfate.硫酸角质素的研究。对陈旧人肋软骨硫酸角质素的甲基化、脱硫及酸水解研究。
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