Seimenis I, Sarafianou A, Papadopoulou H, Papadopoulos Tr
Department of Biomaterials, School of Dentistry, National and Kapodistrian University of Athens, Athens, Greece.
J Oral Rehabil. 2006 Aug;33(8):600-8. doi: 10.1111/j.1365-2842.2005.01599.x.
Composite veneering materials are used as alternatives to porcelain in fixed prosthodontics. Mechanical retention of the resin on the metal framework has been associated with the formation of gaps at the resin/alloy interface, and failure of the restoration. Several chemical bonding systems have been introduced to promote resin adhesion. The purpose of the present study was to evaluate the shear bond strength of three photocured composites (Artglass, Solidex & Signum+) to a Ni-Cr alloy.72 wax disks covered with 150-mum diameter beads were cast and divided in two equal groups. In the first group, Metal Photo Primer was applied on the casting surface, while the Siloc system was used in the second. Each group was divided in three subgroups of 12 samples, in which the three composites were photocured. Half of the specimens of each subgroup were subjected to 1000 and 5000 thermal cycles (5 and 55 degrees C) respectively. All specimens were tested in shear in a universal testing machine. The Siloc-Solidex group showed the highest bond strength (17.3 +/- 3.7 MPa). No statistically significant difference was found between specimens treated with Metal Photo Primer or Siloc. Thermocycling did not significantly affect the bond strength values. Solidex showed an adhesive failure mode for both alloy surface treatments, while Artglass and Signum+ exhibited combination failures. Conclusively, the appropriate alloy surface treatment - resin combination can significantly improve the resin-alloy shear bond strength. Specifically, Solidex resin exhibited significantly higher bond values compared with Artglass and Signum+, for both surface treatments and thermocycling procedures.
复合贴面材料在固定义齿修复中被用作烤瓷材料的替代品。树脂在金属支架上的机械固位与树脂/合金界面间隙的形成以及修复体的失败有关。已经引入了几种化学粘结系统来促进树脂粘结。本研究的目的是评估三种光固化复合材料(Artglass、Solidex和Signum+)与镍铬合金之间的剪切粘结强度。铸造了72个覆盖有直径150微米珠子的蜡盘,并将其分成两组,每组数量相等。在第一组中,在铸件表面涂抹金属光引发剂,而在第二组中使用Siloc系统。每组再分为三个亚组,每组12个样本,分别对三种复合材料进行光固化。每个亚组的一半样本分别经受1000次和5000次热循环(5℃和55℃)。所有样本在万能试验机上进行剪切测试。Siloc-Solidex组显示出最高的粘结强度(17.3±3.7MPa)。在使用金属光引发剂或Siloc处理的样本之间未发现统计学上的显著差异。热循环并未显著影响粘结强度值。对于两种合金表面处理,Solidex均表现出粘结失败模式,而Artglass和Signum+则表现出混合失败模式。总之,合适的合金表面处理 - 树脂组合可以显著提高树脂 - 合金的剪切粘结强度。具体而言,对于两种表面处理和热循环程序,Solidex树脂与Artglass和Signum+相比均表现出显著更高的粘结值。