[黄皮果实挥发油化学成分及微量元素研究]
[Study on chemical constituents of volatile oil and trace elements from fruits of Clausena lansium].
作者信息
Huang Ya-fei, Zhang Yong-ming, Huang Ji-wei, Li Rui-zhen, Liu Jie
机构信息
Pharmacy of the Third Afiliated Hospital, Sun Yat-sen University, Guangzhou 510630, China.
出版信息
Zhongguo Zhong Yao Za Zhi. 2006 Jun;31(11):898-900.
OBJECTIVE
To study and determine the chemical constituents of the volatile oil and the trace elements in the fruits of the Clausena lansium.
METHOD
The essential oils were extracted by supercritical fluid extraction (SFE) and separated on capillary columns with HP6890GC-5973MS. The components were quantitatively determined with normalization method, and were identified with GC-MS. And the trace elements were determined by ICP-MS and ICP-AES.
RESULT
36 Components constituting 95% of the total essential oil were separated and identified, and 11 trace elements were identified.
CONCLUSION
18 Compounds were found from the fruit of C. lansium for the first time.
目的
研究并测定黄皮果实挥发油的化学成分及微量元素。
方法
采用超临界流体萃取法（SFE）提取挥发油，通过HP6890GC - 5973MS在毛细管柱上进行分离。采用归一化法对各成分进行定量测定，并用GC - MS进行成分鉴定。微量元素采用电感耦合等离子体质谱（ICP - MS）和电感耦合等离子体发射光谱（ICP - AES）进行测定。
结果
分离鉴定出占挥发油总量95%的36种成分，鉴定出11种微量元素。
结论
首次从黄皮果实中发现18种化合物。
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