[气相色谱-质谱联用仪测定中毒案件中的东莨菪碱]
[Determination of scopolamine in the poisoning case by GC/MS].
作者信息
Chu Jian-Xin, Xie Yu, Zhuo Xiao-Cong
机构信息
The Procuratorate of Zhejiang Province, Hangzhou 310012, China.
出版信息
Fa Yi Xue Za Zhi. 2006 Aug 15;22(4):285-7.
PMID:17080669
Abstract
OBJECTIVE
To separate and determine scopolamine from the food in a poisoning case by GC/MS.
METHODS
The scopolamine was determined by GC/MS/El used CP5860(CP-sil8CB) column (30 mx 0.25 mmx 0.33 microm) with liquid- liquid extraction.
RESULTS
The deny scopolamine was found in the case sample, and the chromatographic separation of the peaks is fine.
CONCLUSION
The method is accurate and reliable.
摘要
目的
通过气相色谱-质谱联用（GC/MS）法分离并测定一起中毒案件食物中的东莨菪碱。
方法
采用液-液萃取法，以CP5860（CP-sil8CB）柱（30m×0.25mm×0.33μm），通过GC/MS/El测定东莨菪碱。
结果
在案件样本中检出东莨菪碱，各峰色谱分离良好。
结论
该方法准确可靠。
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