Chu Jian-Xin, Xie Yu, Zhuo Xiao-Cong
The Procuratorate of Zhejiang Province, Hangzhou 310012, China.
Fa Yi Xue Za Zhi. 2006 Aug 15;22(4):285-7.
To separate and determine scopolamine from the food in a poisoning case by GC/MS.
The scopolamine was determined by GC/MS/El used CP5860(CP-sil8CB) column (30 mx 0.25 mmx 0.33 microm) with liquid- liquid extraction.
The deny scopolamine was found in the case sample, and the chromatographic separation of the peaks is fine.
The method is accurate and reliable.
通过气相色谱-质谱联用（GC/MS）法分离并测定一起中毒案件食物中的东莨菪碱。
采用液-液萃取法，以CP5860（CP-sil8CB）柱（30m×0.25mm×0.33μm），通过GC/MS/El测定东莨菪碱。
在案件样本中检出东莨菪碱，各峰色谱分离良好。
该方法准确可靠。
