Shahdad Shakeel A, McCabe John F, Bull Steven, Rusby Sandra, Wassell Robert W
Department of Restorative Dentistry, School of Dental Sciences, University of Newcastle upon Tyne, UK.
Dent Mater. 2007 Sep;23(9):1079-85. doi: 10.1016/j.dental.2006.10.001. Epub 2006 Dec 4.
To determine the differences, if any, between hardness measured with traditional Vickers and Martens hardness test methods on denture teeth under 2, 10 and 50 N loads.
Hardness of acrylic resin (VIV), composite resin (ORT) and porcelain (POR) denture tooth materials was measured using a traditional Vickers hardness (HV) method and Martens hardness (HM) method at 2, 10 and 50N test loads. Vickers hardness was also calculated from the force-indentation depth curves (HVfid) that were recorded during Martens hardness. Indentation creep of the three test materials was also determined during Martens hardness testing.
HM values were the same irrespective of the test force used. However, HV values were different for the three test forces. ANOVA using Tukey's test of the HM data showed that the hardness of POR was significantly higher than VIV or ORT (P<0.001). Moreover, ORT had a significantly higher hardness than VIV (P<0.001). The statistical analysis of HVfid data showed similar results. ANOVA of the HV data showed the hardness of VIV to be significantly higher than ORT (P<0.001) under 2, 10 and 50 N test load. The HV values for POR under 2 and 10 N test load could not be calculated because of inability to measure the indentation diagonals. Under the 50 N load, the hardness of POR was significantly higher than VIV and ORT. POR had a significantly lower creep value than any other material tested while VIV showed a statistically significantly higher creep than ORT.
This study confirms that the visco-elastic recovery of the materials has a very significant effect on the outcome of the hardness tests of denture teeth and the Martens hardness test method has obvious advantages when testing dental materials.
确定在2N、10N和50N载荷下,使用传统维氏硬度和马氏硬度测试方法测量义齿牙齿硬度时是否存在差异。
使用传统维氏硬度(HV)法和马氏硬度(HM)法,在2N、10N和50N测试载荷下测量丙烯酸树脂(VIV)、复合树脂(ORT)和瓷(POR)义齿牙齿材料的硬度。还从马氏硬度测试期间记录的力-压痕深度曲线(HVfid)计算维氏硬度。在马氏硬度测试期间还测定了三种测试材料的压痕蠕变。
无论使用何种测试力,HM值均相同。然而,三种测试力下的HV值不同。对HM数据进行Tukey检验的方差分析表明,POR的硬度显著高于VIV或ORT(P<0.001)。此外,ORT的硬度显著高于VIV(P<0.001)。HVfid数据的统计分析显示了类似的结果。HV数据的方差分析表明,在2N、10N和50N测试载荷下,VIV的硬度显著高于ORT(P<0.001)。由于无法测量压痕对角线,因此无法计算2N和10N测试载荷下POR的HV值。在50N载荷下,POR的硬度显著高于VIV和ORT。POR的蠕变值显著低于任何其他测试材料,而VIV的蠕变在统计学上显著高于ORT。
本研究证实材料的粘弹性恢复对义齿牙齿硬度测试结果有非常显著的影响,并且马氏硬度测试方法在测试牙科材料时具有明显优势。