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树脂复合材料不同色调的荧光发射。

Fluorescent emission of varied shades of resin composites.

作者信息

Lim Yong-Kyu, Lee Yong-Keun

机构信息

Department of Orthodontics, Graduate School of Clinical Dentistry, Korea University, Seoul, Republic of Korea.

出版信息

Dent Mater. 2007 Oct;23(10):1262-8. doi: 10.1016/j.dental.2006.11.022. Epub 2006 Dec 29.

Abstract

OBJECTIVES

The objectives of this study were to measure the fluorescent emission and the corresponding color difference by the inclusion and exclusion of the UV component of the standard illuminant D65 of varied shades of commercial resin composites, and to determine the influence of the color parameters and difference in color parameters by the UV component on the color difference caused by the fluorescent emission.

METHOD

Eight light-curing resin composites, a total of 41 shades, were studied. Color and spectral reflectance of specimens, 12 mm in diameter and 1mm in thickness, were measured on a reflection spectrophotometer. An UV filter was adjusted to 100% or 0% location to include or exclude the UV component of the standard illuminant D65. From the spectral reflectance values, subtraction spectrum by the inclusion or exclusion of the UV component was calculated, and fluorescence peak height was determined. Color difference caused by the inclusion or exclusion of the UV component (DeltaE*(ab)-FL) was calculated. Differences in color coordinates (DeltaL*, Deltaa* and Deltab*) by the inclusion or the exclusion of the UV component were calculated.

RESULTS

Fluorescence peak height and DeltaE*(ab)-FL were influenced by the brand and the shade of resin composites and there was a significant interaction between the variables based on two-way ANOVA (p<0.05). DeltaE*(ab)-FL was correlated with the chroma component of the shade, and also with Deltab* [standardized partial correlation coefficient (beta)=-0.699], DeltaL* (beta=0.464) and Deltaa* (beta=0.105) based on multiple regression analyses (p<0.05).

CONCLUSION

Fluorescent emission was influenced by the brand and the shade of resin composites. Fluorescent resin composites showed color shift to blue direction and increased lightness under the UV included illumination.

摘要

目的

本研究的目的是通过纳入和排除不同色调商用树脂复合材料的标准照明体D65的紫外线成分,测量荧光发射和相应的色差,并确定紫外线成分对颜色参数的影响以及颜色参数差异对荧光发射引起的色差的影响。

方法

研究了8种光固化树脂复合材料,共41种色调。在反射分光光度计上测量直径12mm、厚度1mm的试样的颜色和光谱反射率。将紫外线滤光片调整到100%或0%的位置,以纳入或排除标准照明体D65的紫外线成分。根据光谱反射率值,计算纳入或排除紫外线成分后的减法光谱,并确定荧光峰高。计算纳入或排除紫外线成分引起的色差(ΔE*(ab)-FL)。计算纳入或排除紫外线成分时颜色坐标的差异(ΔL*、Δa和Δb)。

结果

荧光峰高和ΔE*(ab)-FL受树脂复合材料的品牌和色调影响,基于双向方差分析,变量之间存在显著交互作用(p<0.05)。基于多元回归分析,ΔE*(ab)-FL与色调的色度成分相关,也与Δb*[标准化偏相关系数(β)=-0.699]、ΔL*(β=0.464)和Δa*(β=0.105)相关(p<0.05)。

结论

荧光发射受树脂复合材料的品牌和色调影响。含荧光的树脂复合材料在包含紫外线的照明下呈现向蓝色方向的颜色偏移和明度增加。

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