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颗粒填料复合材料与不同取向纤维增强复合材料基材之间的粘结强度。

The bond strength of particulate-filler composite to differently oriented fiber-reinforced composite substrate.

作者信息

Lassila Lippo V J, Tezvergil Arzu, Dyer Scott R, Vallittu Pekka K

机构信息

Department of Prosthetic Dentistry and Biomaterials Research, Institute of Dentistry, University of Turku, Turku, Finland.

出版信息

J Prosthodont. 2007 Jan-Feb;16(1):10-7. doi: 10.1111/j.1532-849X.2006.00147.x.

Abstract

PURPOSE

The primary failure mode of fiber-reinforced composite (FRC) materials used intraorally is delamination or debonding of particulate filler composite (PFC), the esthetic veneer, from the underlying FRC framework. The objective of the current study was to evaluate the effect of unidirectional fiber orientation and load direction on the shear bond strength of PFC to FRC.

MATERIALS AND METHODS

Unidirectional E-glass FRC was used as an adhesion substrate for the PFC. E-glass FRCs were oriented in three ways--Group A: in the plane perpendicular to the bonding surface; Group B: along the bonding surface longitudinal to the load; and Group C: along the bonding surface, transverse to the load. The FRC substrates were ground flat with 1200 grit. The PFC adherend was bonded to FRC using an intermediate resin. Twelve specimens for each group were water stored (37 degrees C) for 3 days before a shear bond strength test was conducted.

RESULTS

A one-way analysis of variance showed that the direction of the applied load to the fiber direction had a significant effect on the bond strength values (p < 0.001). A Weibull analysis produced values (characteristic strength and Weibull modulus) of Group A (46.5 MPa, 12.1), Group B (40.6 MPa, 4.6), and Group C (27.6 MPa, 3.5).

SIGNIFICANCE

The highest shear bond strength values and Weibull modulus were obtained when the fibers were oriented perpendicular to the bonding surface, exposing the fiber ends to the PFC. Interface strategies between hybrid composite layers may be developed to exploit anisotropic behavior in the adherence between FRC and PFC.

摘要

目的

口腔内使用的纤维增强复合材料(FRC)的主要失效模式是颗粒填料复合材料(PFC)美学贴面与底层FRC框架之间的分层或脱粘。本研究的目的是评估单向纤维取向和载荷方向对PFC与FRC剪切粘结强度的影响。

材料与方法

单向E玻璃FRC用作PFC的粘结基底。E玻璃FRC有三种取向方式——A组:在垂直于粘结表面的平面内;B组:沿粘结表面纵向于载荷方向;C组:沿粘结表面横向于载荷方向。FRC基底用1200目砂纸磨平。使用中间树脂将PFC被粘物粘结到FRC上。每组12个试样在37℃水中储存3天,然后进行剪切粘结强度测试。

结果

单向方差分析表明,施加于纤维方向的载荷方向对粘结强度值有显著影响(p < 0.001)。威布尔分析得出A组(46.5 MPa,12.1)、B组(40.6 MPa,4.6)和C组(27.6 MPa,3.5)的值(特征强度和威布尔模量)。

意义

当纤维垂直于粘结表面取向,使纤维末端暴露于PFC时,可获得最高的剪切粘结强度值和威布尔模量。可开发混合复合层之间的界面策略,以利用FRC与PFC粘结中的各向异性行为。

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