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硅烷化对纤维桩与各种树脂水门汀粘结强度的影响。

Effect of silanization on bond strengths of fiber posts to various resin cements.

作者信息

Bitter Kerstin, Noetzel Jörn, Neumann Konrad, Kielbassa Andrej M

机构信息

Department of Operative Dentistry and Periodontology, University School of Dental Medicine, Campus Benjamin Franklin, Charité-Universitätsmedizin Berlin, Germany.

出版信息

Quintessence Int. 2007 Feb;38(2):121-8.

Abstract

OBJECTIVES

To investigate the effects of pretreatment (silanization) on bond strengths between 3 different types of fiber posts and 4 resin cements, respectively.

METHOD AND MATERIALS

Prefabricated quartz-fiber (Unicore Post, Ultradent) and prefabricated glass-fiber (FRC Postec, Ivoclar Vivadent) posts with a cross-linked polymer matrix and individually formed glass-fiber posts with an interpenetrating polymer network (IPN Post, Stick Tech) (n = 160 each) were inserted into resin composite disks (2 mm thick) using the following resin cements and silane solutions: Panavia F/Porcelain Bond Activator (Kuraray), PermaFlo DC/Silane (Ultradent), Variolink II/Monobond S (Ivoclar Vivadent) and RelyX Unicem/Espe Sil (3M Espe). Nonsilanated posts served as controls. The push-out bond strengths were determined before (n = 10) and after (n = 10) thermocycling (2,000 cycles, 5 degrees C to 55 degrees C, dwelling time 30 seconds).

RESULTS

Bond strengths (mean [SD]) were significantly affected by the resin cement (P < .001), the pretreatment (P < .001), and the type of post (P < .001), but not by thermocycling (P = .955, 4-way ANOVA). The IPN post demonstrated significantly higher bond strengths compared to the other posts (P < .05; Tukey B). Silanization significantly increased bond strengths (15.2 [5.2] MPa) compared to those of the control groups (13.9 [4.9] MPa).

CONCLUSION

The type of fiber post revealed a significant influence on bond strengths, whereas the effects of silanization appeared to be clinically negligible.

摘要

目的

分别研究预处理(硅烷化)对3种不同类型纤维桩与4种树脂水门汀之间粘结强度的影响。

方法和材料

将预制石英纤维桩(Unicore Post,Ultradent)、预制玻璃纤维桩(FRC Postec,Ivoclar Vivadent)(具有交联聚合物基质)以及单独成型的具有互穿聚合物网络的玻璃纤维桩(IPN Post,Stick Tech)(各n = 160),使用以下树脂水门汀和硅烷溶液插入树脂复合盘(2 mm厚)中:Panavia F/瓷粘结活化剂(可乐丽)、PermaFlo DC/硅烷(Ultradent)、Variolink II/Monobond S(Ivoclar Vivadent)和RelyX Unicem/Espe Sil(3M Espe)。未进行硅烷化处理的桩作为对照。在热循环(2000次循环,5℃至55℃, dwell时间30秒)之前(n = 10)和之后(n = 10)测定推出粘结强度。

结果

粘结强度(均值[标准差])受到树脂水门汀(P < 0.001)、预处理(P < 0.001)和桩的类型(P < 0.001)的显著影响,但不受热循环的影响(P = 0.955,四因素方差分析)。与其他桩相比,IPN桩表现出显著更高的粘结强度(P < 0.05;Tukey B检验)。与对照组(13.9 [4.9] MPa)相比,硅烷化显著提高了粘结强度(15.2 [5.2] MPa)。

结论

纤维桩的类型对粘结强度有显著影响,而硅烷化的影响在临床上似乎可以忽略不计。

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