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表面粗糙度对树脂复合材料和玻璃陶瓷材料机械强度的影响。

Influence of surface roughness on mechanical strength of resin composite versus glass ceramic materials.

作者信息

Lohbauer Ulrich, Müller Frank A, Petschelt Anselm

机构信息

Dental Clinic 1, Operative Dentistry and Periodontology, University of Erlangen-Nuremberg, Glückstr. 11, D-91054 Erlangen, Germany.

出版信息

Dent Mater. 2008 Feb;24(2):250-6. doi: 10.1016/j.dental.2007.05.006. Epub 2007 Jul 12.

Abstract

OBJECTIVES

Clinical polishing leads to reduction of surface flaws sizes and thus to increased mechanical strength. The aim of the present work was to assess fracture strength of a resin composite and of a glass ceramic as a function of surface roughness and to relate the strength data to flaw sizes, microstructural and fractographic examinations.

METHODS

Specimens have manufactured out of a resin composite (Tetric EvoCeram, TEC) and out of glass ceramic material (IPS E.max Press, EMP). Different surface roughness levels have been induced using cutting, grinding and polishing techniques and quantified under CLSM. Fracture strength was measured in four-point bending and analyzed using Weibull statistics. Indentation fracture method was used to calculate fracture toughness. Critical flaw sizes were calculated and related to microstructure. Microstructural and fractographic examinations have been performed under SEM.

RESULTS

Fracture strength upon the glass ceramic material decreased from 441.4 to 303.3 MPa (R(a)=150 nm-1.5 microm) and upon the resin composite from 109.8 to 74.0 MPa (R(a)=300 nm-50 microm). EMP exhibited a fracture toughness of K(Ic)=4.14 MPam(0.5) and TEC of K(Ic)=1.89 MPam(0.5). Calculated crack lengths for EMP ranged from 28.1 microm (441.4 MPa) to 59.6 microm (303.3 MPa) and for TEC from 94.3 microm (109.8 MPa) to 207.0 microm (74.0 MPa).

SIGNIFICANCE

Dependency of fracture strength on surface roughness is neither determined by crystallite size of the glass ceramic material nor by filler sizes of the resin composite. No significant increase in fracture strength has been observed below 0.65 microm (1000 grit) in EMP. For TEC a threshold value might be determined below 2.1 microm (320 grit). Optimal polishing of a restoration right after placement is strongly recommended to keep an optimum strength performance through the whole clinical lifetime.

摘要

目的

临床打磨可减小表面缺陷尺寸,从而提高机械强度。本研究的目的是评估树脂复合材料和玻璃陶瓷的断裂强度与表面粗糙度的关系,并将强度数据与缺陷尺寸、微观结构和断口形貌检查相关联。

方法

用树脂复合材料(Tetric EvoCeram,TEC)和玻璃陶瓷材料(IPS E.max Press,EMP)制作试样。使用切割、研磨和抛光技术产生不同的表面粗糙度水平,并在共聚焦激光扫描显微镜下进行量化。在四点弯曲试验中测量断裂强度,并使用威布尔统计分析。采用压痕断裂法计算断裂韧性。计算临界缺陷尺寸并将其与微观结构相关联。在扫描电子显微镜下进行微观结构和断口形貌检查。

结果

玻璃陶瓷材料的断裂强度从441.4MPa降至303.3MPa(R(a)=150nm - 1.5μm),树脂复合材料的断裂强度从109.8MPa降至74.0MPa(R(a)=300nm - 50μm)。EMP的断裂韧性为K(Ic)=4.14MPam(0.5),TEC的断裂韧性为K(Ic)=1.89MPam(0.5)。EMP计算出的裂纹长度范围为28.1μm(441.4MPa)至59.6μm(303.3MPa),TEC的裂纹长度范围为94.3μm(109.8MPa)至207.0μm(74.0MPa)。

意义

断裂强度对表面粗糙度的依赖性既不是由玻璃陶瓷材料的微晶尺寸决定的,也不是由树脂复合材料的填料尺寸决定的。在EMP中,低于0.65μm(1000目)时未观察到断裂强度有显著增加。对于TEC,阈值可能在2.1μm(320目)以下确定。强烈建议在修复体就位后立即进行最佳打磨,以在整个临床使用期内保持最佳强度性能。

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