Xie Xiao-xia, Ge Fa-huan
Zhongshan University, Guangzhou 510275, China.
Zhong Yao Cai. 2007 Mar;30(3):345-9.
The extraction of fatty oils from the seed of Akebia trifoliata (Thunb) Koidz with supercritical CO2 was studied. The effects of extraction pressure, extraction temperature on the yields were discussed. The optimal condition of this method was as follow: extraction pressure 30 MPa, extraction temerature 45 degrees C, separator I pressure 11 MPa, separator I temperature 50 degrees C, separator II pressure 6MPa, separator II temperature 45 degrees C, extraction period 2 hours. Compared with the traditional solvent extraction, with a GC-MS analysis, it revealed that the component extracted with supercritical CO2 was basically consistent with that extracted with petroleum ether, and it was rich unsaturated fatty acid.
研究了用超临界CO₂从三叶木通(Thunb)Koidz种子中提取油脂。讨论了萃取压力、萃取温度对产率的影响。该方法的最佳条件如下:萃取压力30MPa,萃取温度45℃,分离器I压力11MPa,分离器I温度50℃,分离器II压力6MPa,分离器II温度45℃,萃取时间2小时。与传统溶剂萃取相比,通过气相色谱-质谱联用分析表明,超临界CO₂萃取的成分与石油醚萃取的基本一致,且富含不饱和脂肪酸。