13C-13C chemical shift correlation in rotating solids without 1H decoupling during mixing.

作者信息

Herbst Christian, Riedel Kerstin, Leppert Jörg, Ohlenschläger Oliver, Görlach Matthias, Ramachandran Ramadurai

机构信息

Molecular Biophysics/NMR spectroscopy Leibniz Institute for Age Research, Fritz Lipmann Institute, Beutenbergstrasse 11, 07745 Jena, Germany.

出版信息

Chemphyschem. 2007 Aug 24;8(12):1770-3. doi: 10.1002/cphc.200700234.

DOI:10.1002/cphc.200700234

PMID:17665381

Abstract

摘要

相似文献

13C-13C chemical shift correlation in rotating solids without 1H decoupling during mixing.

Chemphyschem. 2007 Aug 24;8(12):1770-3. doi: 10.1002/cphc.200700234.

The effectiveness of 1H decoupling in the 13C MAS NMR of paramagnetic solids: an experimental case study incorporating copper(II) amino acid complexes.1H去耦在顺磁性固体的13C MAS NMR中的有效性：一个包含铜（II）氨基酸配合物的实验案例研究。

J Magn Reson. 2008 Mar;191(1):31-46. doi: 10.1016/j.jmr.2007.11.012. Epub 2007 Nov 28.

Trace level detection of compounds related to the chemical weapons convention by 1H-detected 13C NMR spectroscopy executed with a sensitivity-enhanced, cryogenic probehead.使用灵敏度增强的低温探头通过1H检测的13C核磁共振光谱法对与《化学武器公约》相关的化合物进行痕量检测。

Anal Chem. 2008 Apr 15;80(8):3000-6. doi: 10.1021/ac7021053. Epub 2008 Mar 18.

High-resolution 14N-edited 1H-13C correlation NMR experiment to study biological solids.用于研究生物固体的高分辨率14N编辑的1H-13C相关核磁共振实验。

J Magn Reson. 2008 Oct;194(2):317-20. doi: 10.1016/j.jmr.2008.07.021. Epub 2008 Jul 29.

A joined theoretical-experimental investigation on the 1H and 13C NMR signatures of defects in poly(vinyl chloride).一项关于聚氯乙烯中缺陷的1H和13C NMR特征的理论与实验联合研究。

J Phys Chem B. 2008 Nov 27;112(47):14804-18. doi: 10.1021/jp805676q.

Chemical shift correlation NMR spectroscopy with indirect detection in fast rotating solids: studies of organically functionalized mesoporous silicas.

J Am Chem Soc. 2007 Oct 10;129(40):12076-7. doi: 10.1021/ja074746+. Epub 2007 Sep 18.

Incorporating 1H chemical shift determination into 13C-direct detected spectroscopy of intrinsically disordered proteins in solution.将¹H化学位移测定纳入溶液中内在无序蛋白质的¹³C直接检测光谱法。

J Magn Reson. 2009 Oct;200(2):354-8. doi: 10.1016/j.jmr.2009.07.014. Epub 2009 Jul 17.

Binuclear spin state selective detection of 1H single quantum transitions using triple quantum coherence: a novel method for enantiomeric discrimination.利用三量子相干对1H单量子跃迁进行双核自旋态选择性检测：一种对映体鉴别新方法。

J Magn Reson. 2008 May;192(1):92-100. doi: 10.1016/j.jmr.2008.02.006. Epub 2008 Feb 12.

DFT calculations of 1H and 13C NMR chemical shifts in transition metal hydrides.过渡金属氢化物中氢-1和碳-13核磁共振化学位移的密度泛函理论计算

Dalton Trans. 2008 Aug 14(30):3959-70. doi: 10.1039/b802190b. Epub 2008 May 7.

Radio frequency-driven recoupling at high magic-angle spinning frequencies: homonuclear recoupling sans heteronuclear decoupling.高魔角旋转频率下的射频驱动再耦合：无需异核去耦的同核再耦合

J Chem Phys. 2008 Feb 7;128(5):052321. doi: 10.1063/1.2834736.

引用本文的文献

Simplified Preservation of Equivalent Pathways Spectroscopy.等效路径光谱的简化保存

JACS Au. 2023 Oct 11;3(10):2763-2771. doi: 10.1021/jacsau.3c00312. eCollection 2023 Oct 23.

Optimization of band-selective homonuclear dipolar recoupling in solid-state NMR by a numerical phase search.通过数值相位搜索优化固态核磁共振中的带选择性同核偶极重耦合

J Chem Phys. 2019 Apr 21;150(15):154201. doi: 10.1063/1.5092986.

Design of high-power, broadband 180 degrees pulses and mixing sequences for fast MAS solid state chemical shift correlation NMR spectroscopy.用于快速MAS固态化学位移相关核磁共振光谱的高功率宽带180度脉冲和混合序列设计。

J Biomol NMR. 2009 Jan;43(1):51-61. doi: 10.1007/s10858-008-9292-9. Epub 2008 Nov 19.

文献检索

告别复杂PubMed语法，用中文像聊天一样搜索，搜遍4000万医学文献。AI智能推荐，让科研检索更轻松。

立即免费搜索

文件翻译

保留排版，准确专业，支持PDF/Word/PPT等文件格式，支持 12+语言互译。

免费翻译文档

深度研究

AI帮你快速写综述，25分钟生成高质量综述，智能提取关键信息，辅助科研写作。

立即免费体验