Gregoire John M, van Dover R B, Jin Jing, Disalvo Francis J, Abruña Héctor D
Department of Physics, Cornell University, Ithaca, New York 14853, USA.
Rev Sci Instrum. 2007 Jul;78(7):072212. doi: 10.1063/1.2755967.
We describe a sputtering system that can deposit composition spreads in an effectively UHV environment but which does not require the high-throughput paradigm to be compromised by a long pump down each time a target is changed. The system deploys four magnetron sputter guns in a cryoshroud (getter sputtering) which allows elements such as Ti and Zr to be deposited with minimal contamination by oxygen or other reactive background gases. The system also relies on custom substrate heaters to give rapid heating and cool down. The effectiveness of the gettering technique is evaluated, and example results obtained for catalytic activity of a pseudoternary composition spread are presented.