Rubin J R, Haromy T P, Sundaralingam M
NCI-FCRF, Frederick, MD 21701.
Acta Crystallogr C. 1991 Aug 15;47 ( Pt 8):1712-4. doi: 10.1107/s010827019100032x.
[Rh2(C2H3O2)4(C11H16N5O4)2].H2O, Mr = 1024.6, triclinic, P1, a = 7.808 (3), b = 11.469 (4), c = 12.091 (2) A, alpha = 69.55 (2), beta = 79.46 (2), gamma = 76.61 (3) degrees, V = 980.7 (6) A3, Z = 1, Dx = 1.735 g cm-3, lambda (Cu K alpha) = 1.5418 A, mu = 77.6 cm-1, F(000) = 522, room temperature, R = 0.053 for 3638 unique reflections. Structure consists of two rhodium(II) ions in a metal--metal bond bridged by four acetate groups. The remaining axial coordination sites on the rhodium ions are coordinated to the N(7) positions of two 1-methyladenosine molecules.
[Rh₂(C₂H₃O₂)₄(C₁₁H₁₆N₅O₄)₂]·H₂O，Mr = 1024.6，三斜晶系，P1，a = 7.808(3)，b = 11.469(4)，c = 12.091(2) Å，α = 69.55(2)，β = 79.46(2)，γ = 76.61(3)°，V = 980.7(6) ų，Z = 1，Dx = 1.735 g cm⁻³，λ(Cu Kα) = 1.5418 Å，μ = 77.6 cm⁻¹，F(000) = 522，室温，对于3638个独立反射，R = 0.053。结构由两个通过四个乙酸根基团桥连形成金属 - 金属键的铑(II)离子组成。铑离子上其余的轴向配位点与两个1 - 甲基腺苷分子的N(7)位置配位。
