Kahveci Bahittin
Department of Chemistry, Rize Faculty of Arts and Science, Karadeniz Technical University, 53100, Rize, Turkey.
Molecules. 2005 Feb 28;10(2):376-82. doi: 10.3390/10020376.
Iminoester hydrochlorides 1 have been synthesized. These compounds were then converted into ester ethoxycarbonyl hydrazones 2, from which in turn a new series of substituted 4-amino-4,5-dihydro-1H-1,2,4-triazole-5-ones, 3, was then prepared. Finally a set of isatin imine derivatives 4 was obtained from the reaction of compounds 3 with isatin. The structures of all the new synthesized compounds were confirmed by elemental analyses, IR, (1)H-NMR and (13)C-NMR spectra.
已合成盐酸亚胺酯1。然后将这些化合物转化为酯乙氧羰基腙2,进而由其制备了一系列新的取代4-氨基-4,5-二氢-1H-1,2,4-三唑-5-酮3。最后,通过化合物3与异吲哚酮的反应得到了一组异吲哚酮亚胺衍生物4。所有新合成化合物的结构均通过元素分析、红外光谱、(1)H-NMR和(13)C-NMR光谱得以确证。