含苯并-15-冠-5部分的新型席夫碱的合成与光谱表征
Synthesis and spectroscopic characterization of new Schiff bases containing the benzo-15-crown-5 moiety.
作者信息
Hayvali Zeliha, Hayvali Mustafa, Dal Hakan
机构信息
Ankara University, Department of Chemistry, Faculty of Science, 06100, Tandoğan, Ankara, Turkey.
出版信息
Molecules. 2004 Sep 30;9(10):860-6. doi: 10.3390/91000860.
Abstract
New crown ether Schiff base derivatives were prepared by the condensation of 4'-formylbenzo-15-crown-5 or 4'-formyl-5'-hydroxybenzo-15-crown-5 with 1,2-bis(2-aminophenoxy)ethane. The structures of these new compounds were confirmed on the basis of elemental analysis, IR, (1)H- and (13)C-NMR, UV-Vis and mass spectroscopic data.
摘要
通过4'-甲酰基苯并-15-冠-5或4'-甲酰基-5'-羟基苯并-15-冠-5与1,2-双(2-氨基苯氧基)乙烷缩合制备了新型冠醚席夫碱衍生物。基于元素分析、红外光谱、(1)H-和(13)C-核磁共振、紫外可见光谱和质谱数据确定了这些新化合物的结构。
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