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储存时长对硅酮基和丙烯酸树脂基弹性义齿衬垫与加工后的义齿基托丙烯酸树脂之间的硬度及拉伸粘结强度的影响

Effect of storage duration on the hardness and tensile bond strength of silicone- and acrylic resin-based resilient denture liners to a processed denture base acrylic resin.

作者信息

Mese Ayse, Guzel Kahraman G

机构信息

Department of Prosthodontics, Dicle University, Dental Faculty, Diyarbakir, Turkey.

出版信息

J Prosthet Dent. 2008 Feb;99(2):153-9. doi: 10.1016/S0022-3913(08)60032-3.

Abstract

STATEMENT OF PROBLEM

Two potential problems commonly identified with a denture base incorporating a resilient liner are a failure of the bond between the acrylic resin and resilient liner material and a loss of resiliency of the resilient liner material over time.

PURPOSE

This investigation evaluated the effect of storage duration on the tensile bond strength and hardness of acrylic resin- and silicone-based resilient liners that were either heat- or autopolymerized onto denture base acrylic resin.

MATERIAL AND METHODS

The denture liners investigated were a definitive acrylic resin-based heat-polymerized (Vertex Soft), interim acrylic resin-based autopolymerized (Coe-Soft), definitive silicone-based heat-polymerized (Molloplast-B), and definitive silicone-based autopolymerized (Mollosil Plus) resilient liner. The resilient liners were processed according to manufacturers' instructions. The resilient liner specimens for tensile bond strength testing (n=10) were 10 x 10 x 3 mm and were processed between 2 polymethyl methacrylate (PMMA) (Meliodent) blocks (40 x 10 x 10 mm). The resilient liner specimens for hardness testing (n=10) were 20 mm in diameter and 12 mm in height. Specimen shape and liner thickness were standardized. Specimens were stored for 1 day, 1 week, or 1, 3, or 6 months in water at 37 degrees C. Tensile bond strength was measured in a universal testing machine at a crosshead speed of 20 mm/min, and hardness was measured using a Shore A durometer. Two-way ANOVA and Tukey HSD tests were used to analyze the data (alpha=.05).

RESULTS

The results indicated that there were significant differences both in the hardness and bond strength values of resilient liner materials. The definitive silicone-based heat-polymerized (Molloplast-B) resilient liner had significantly higher bond strength and lower hardness values than the others. Prolonged exposure to water produced significantly higher hardness values and lower bond strength values.

CONCLUSIONS

Within the limitations of this in vitro study, specimens of resilient liners immersed in water demonstrated significantly (P<.001) lower bond strength values and higher hardness values over time.

摘要

问题陈述

在带有弹性衬层的义齿基托中,通常会发现两个潜在问题,即丙烯酸树脂与弹性衬层材料之间的粘结失败以及弹性衬层材料随时间推移弹性丧失。

目的

本研究评估了储存时间对通过热聚合或自聚合方式附着在义齿基托丙烯酸树脂上的丙烯酸树脂基和硅树脂基弹性衬层的拉伸粘结强度和硬度的影响。

材料与方法

所研究的义齿衬层包括一种定制的丙烯酸树脂基热聚合衬层(Vertex Soft)、一种临时的丙烯酸树脂基自聚合衬层(Coe-Soft)、一种定制的硅树脂基热聚合衬层(Molloplast-B)和一种定制的硅树脂基自聚合衬层(Mollosil Plus)。弹性衬层按照制造商的说明进行加工。用于拉伸粘结强度测试的弹性衬层试样(n = 10)尺寸为10×10×3毫米,在两块聚甲基丙烯酸甲酯(PMMA)(Meliodent)块体(40×10×10毫米)之间加工而成。用于硬度测试的弹性衬层试样(n = 10)直径为20毫米,高度为12毫米。试样形状和衬层厚度标准化。试样在37℃的水中储存1天、1周或1、3或6个月。在万能试验机上以20毫米/分钟的十字头速度测量拉伸粘结强度,使用邵氏A硬度计测量硬度。采用双向方差分析和Tukey HSD检验分析数据(α = 0.05)。

结果

结果表明,弹性衬层材料的硬度和粘结强度值均存在显著差异。定制的硅树脂基热聚合衬层(Molloplast-B)的粘结强度明显高于其他衬层,硬度值则低于其他衬层。长时间接触水会使硬度值显著升高,粘结强度值显著降低。

结论

在本体外研究的局限性范围内,浸泡在水中的弹性衬层试样随时间推移粘结强度值显著降低(P < 0.001),硬度值显著升高。

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