• 文献检索
  • 文档翻译
  • 深度研究
  • 学术资讯
  • Suppr Zotero 插件Zotero 插件
  • 邀请有礼
  • 套餐&价格
  • 历史记录
应用&插件
Suppr Zotero 插件Zotero 插件浏览器插件Mac 客户端Windows 客户端微信小程序
定价
高级版会员购买积分包购买API积分包
服务
文献检索文档翻译深度研究API 文档MCP 服务
关于我们
关于 Suppr公司介绍联系我们用户协议隐私条款
关注我们

Suppr 超能文献

核心技术专利:CN118964589B侵权必究
粤ICP备2023148730 号-1Suppr @ 2026

文献检索

告别复杂PubMed语法,用中文像聊天一样搜索,搜遍4000万医学文献。AI智能推荐,让科研检索更轻松。

立即免费搜索

文件翻译

保留排版,准确专业,支持PDF/Word/PPT等文件格式,支持 12+语言互译。

免费翻译文档

深度研究

AI帮你快速写综述,25分钟生成高质量综述,智能提取关键信息,辅助科研写作。

立即免费体验

超声促进下Zr(acac)₄在环境条件下催化绿色合成2,4,5-三取代咪唑

Ultrasound-promoted greener synthesis of 2,4,5-trisubstituted imidazoles catalyzed by Zr(acac)4 under ambient conditions.

作者信息

Khosropour Ahmad R

机构信息

Catalysis Division, Department of Chemistry, University of Isfahan, Hezar Jerib Street, Isfahan 81746-73441, Iran.

出版信息

Ultrason Sonochem. 2008 Jul;15(5):659-64. doi: 10.1016/j.ultsonch.2007.12.005. Epub 2008 Jan 12.

DOI:10.1016/j.ultsonch.2007.12.005
PMID:18299244
Abstract

A simple, efficient and green procedure has been developed for the synthesis of 2,4,5-trisubstituted imidazoles catalyzed by zirconium (IV) acetylacetonate using ultrasonic irradiation. The present methodology offers several advantages such as excellent yields, simple procedure, short reaction times and milder conditions.

摘要

已开发出一种简单、高效且绿色的方法,用于在超声辐射下由乙酰丙酮锆(IV)催化合成2,4,5-三取代咪唑。该方法具有诸多优点,如产率优异、步骤简单、反应时间短且条件更温和。

相似文献

1
Ultrasound-promoted greener synthesis of 2,4,5-trisubstituted imidazoles catalyzed by Zr(acac)4 under ambient conditions.超声促进下Zr(acac)₄在环境条件下催化绿色合成2,4,5-三取代咪唑
Ultrason Sonochem. 2008 Jul;15(5):659-64. doi: 10.1016/j.ultsonch.2007.12.005. Epub 2008 Jan 12.
2
Ultrasound-promoted greener synthesis of aryl-14-H-dibenzo[a,j]xanthenes catalyzed by NH4H2PO4/SiO2 in water.超声促进磷酸二氢铵/二氧化硅在水中催化芳基-14-H-二苯并[a,j]呫吨的绿色合成
Ultrason Sonochem. 2009 Jan;16(1):7-10. doi: 10.1016/j.ultsonch.2008.05.010. Epub 2008 May 24.
3
Ultrasound-promoted greener synthesis of 2H-chromen-2-ones catalyzed by copper perchlorate in solventless media.超声促进高氯酸铜在无溶剂介质中催化绿色合成2H-色烯-2-酮
Ultrason Sonochem. 2009 Aug;16(6):705-7. doi: 10.1016/j.ultsonch.2009.04.002. Epub 2009 Apr 14.
4
Ultrasound-promoted greener synthesis of benzoheterocycle derivatives catalyzed by nanocrystalline copper(II) oxide.超声促进纳米晶氧化铜催化的苯并杂环衍生物的绿色合成。
Ultrason Sonochem. 2010 Jun;17(5):764-7. doi: 10.1016/j.ultsonch.2010.01.017. Epub 2010 Feb 12.
5
Ultrasound-promoted synthesis of oximes catalyzed by a basic ionic liquid [bmIm]OH.碱性离子液体[bmIm]OH催化超声促进肟的合成。
Ultrason Sonochem. 2009 Mar;16(3):301-3. doi: 10.1016/j.ultsonch.2008.09.003. Epub 2008 Sep 26.
6
A highly efficient magnetic solid acid catalyst for synthesis of 2,4,5-trisubstituted imidazoles under ultrasound irradiation.一种在超声辐射下高效合成 2,4,5-三取代咪唑的磁性固体酸催化剂。
Ultrason Sonochem. 2013 Mar;20(2):740-6. doi: 10.1016/j.ultsonch.2012.10.004. Epub 2012 Oct 17.
7
Ultrasound promoted selective synthesis of 2-aryl-5,6-dihydro-4H-1,3-oxazines catalyzed by K-10 and KSF montmorillonite clays: a practical procedure under mild and solvent-free conditions.超声促进 K-10 和 KSF 蒙脱石黏土催化的 2-芳基-5,6-二氢-4H-1,3-恶嗪的选择性合成:温和无溶剂条件下的实用方法。
Ultrason Sonochem. 2010 Jun;17(5):857-62. doi: 10.1016/j.ultsonch.2010.02.005. Epub 2010 Feb 11.
8
Ionic liquid [EMIM]OAc under ultrasonic irradiation towards the first synthesis of trisubstituted imidazoles.超声辐射下离子液体 [EMIM]OAc 促进的三取代咪唑的首次合成。
Ultrason Sonochem. 2010 Jun;17(5):749-51. doi: 10.1016/j.ultsonch.2010.01.015. Epub 2010 Feb 4.
9
Ultrasound-assisted synthesis of pyrroles catalyzed by zirconium chloride under solvent-free conditions.无溶剂条件下氯化锆催化超声辅助合成吡咯
Ultrason Sonochem. 2008 Jul;15(5):673-6. doi: 10.1016/j.ultsonch.2008.02.008. Epub 2008 Feb 26.
10
Ultrasound-promoted a green protocol for the synthesis of 2,4-diarylthiazoles under ambient temperature in [bmim]BF(4).超声促进的在室温下于[bmim]BF(4)中合成2,4-二芳基噻唑的绿色方法。
Ultrason Sonochem. 2009 Aug;16(6):711-7. doi: 10.1016/j.ultsonch.2009.04.001. Epub 2009 Apr 12.

引用本文的文献

1
Copper borate (CuBO)-promoted multi-component green synthesis of 2,4,5-triarylimidazole derivatives and evidence of conversion of copper borate (CuBO) into Cu(OAc) in the presence of NHOAc.硼酸铜(CuBO)促进的2,4,5-三芳基咪唑衍生物的多组分绿色合成以及在NHOAc存在下硼酸铜(CuBO)转化为醋酸铜(Cu(OAc))的证据。
RSC Adv. 2023 Jul 4;13(29):19846-19855. doi: 10.1039/d3ra03183g. eCollection 2023 Jun 29.
2
Synthesis of Imidazole-Based Molecules under Ultrasonic Irradiation Approaches.超声辐射法合成咪唑类分子的方法研究。
Molecules. 2023 Jun 19;28(12):4845. doi: 10.3390/molecules28124845.
3
Preparation of polysubstituted imidazoles using AC-SOH/[Urea][ZnCl] as an efficient catalyst system: a novel method, and α-glucosidase inhibitor activity.
以AC-SOH/[尿素][ZnCl]为高效催化剂体系制备多取代咪唑:一种新方法及α-葡萄糖苷酶抑制活性
RSC Adv. 2023 Apr 20;13(18):12455-12463. doi: 10.1039/d3ra00755c. eCollection 2023 Apr 17.
4
Synthesis, antioxidant activity, antimicrobial efficacy and molecular docking studies of 4-chloro-2-(1-(4-methoxyphenyl)-4,5-diphenyl-1-imidazol-2-yl)phenol and its transition metal complexes.4-氯-2-(1-(4-甲氧基苯基)-4,5-二苯基-1-咪唑-2-基)苯酚及其过渡金属配合物的合成、抗氧化活性、抗菌功效和分子对接研究
RSC Adv. 2023 Mar 21;13(14):9222-9230. doi: 10.1039/d2ra08327b. eCollection 2023 Mar 20.
5
Ionic Liquid Solvation versus Catalysis: Computational Insight from a Multisubstituted Imidazole Synthesis in [EtNH][HSO].离子液体溶剂化与催化作用:来自在[EtNH][HSO]中多取代咪唑合成的计算洞察。
ChemistryOpen. 2016 Aug 17;5(5):460-469. doi: 10.1002/open.201600066. eCollection 2016 Oct.
6
Synthesis and physicochemical properties of novel lophine derivatives as chemiluminescent in vitro activators for detection of free radicals.
Eur Biophys J. 2015 Dec;44(8):623-34. doi: 10.1007/s00249-015-1056-3. Epub 2015 Jul 30.
7
Wells-Dawson heteropolyacid supported on silica: a highly efficient catalyst for synthesis of 2,4,5-trisubstituted and 1,2,4,5-tetrasubstituted imidazoles.负载在二氧化硅上的 Wells-Dawson 杂多酸:一种高效合成 2,4,5-三取代和 1,2,4,5-四取代咪唑的催化剂。
Mol Divers. 2010 Nov;14(4):635-41. doi: 10.1007/s11030-009-9197-x. Epub 2009 Oct 29.