Taira Yohsuke, Kamada Kohji, Atsuta Mitsuru
Division of Applied Prosthodontics, Graduate School of Biomedical Sciences, Nagasaki University, 1-7-1 Sakamoto, Nagasaki 852-8588, Japan.
Dent Mater J. 2008 Jan;27(1):69-74. doi: 10.4012/dmj.27.69.
The purpose of the present study was to evaluate the effects of four experimental primers on bond strength between a self-curing luting agent and silver-palladium-gold alloy. The experimental primers were in mixed solutions of a thiouracil primer (Metaltite) and a phosphate primer (Epricord, PM, PE, or PP), which were designated as Metaltite/Epricord, Metaltite/PM, Metaltite/PE, and Metaltite/PP respectively. Three primers (Metal Primer II, V-Primer, and Alloy Primer) were also prepared as controls. Alumina-blasted metal alloys were bonded with acrylic rods. After 5,000 thermocycles, the maximum shear bond strength was obtained with Metaltite/PE (27.8+/-2.4 MPa) and Metaltite/Epricord (27.6+/-5.9 MPa), followed by Metaltite/PP, Alloy Primer, Metaltite, Metaltite/PM, Metal Primer II, V-Primer, and Epricord. PE, PM, and PP showed the lowest bond strength. Results of this study revealed that the combined use of a thiouracil monomer and a phosphate monomer improved adhesive bonding. In this light, clinicians should pay attention to the types of functional monomers dissolved in a primer when fabricating resin-bonded prostheses.
本研究的目的是评估四种实验性底漆对自固化粘接剂与银钯金合金之间粘接强度的影响。实验性底漆为硫脲底漆(Metaltite)与磷酸盐底漆(Epricord、PM、PE或PP)的混合溶液,分别命名为Metaltite/Epricord、Metaltite/PM、Metaltite/PE和Metaltite/PP。还制备了三种底漆(金属底漆II、V-底漆和合金底漆)作为对照。用丙烯酸棒对经氧化铝喷砂处理的金属合金进行粘接。经过5000次热循环后,Metaltite/PE(27.8±2.4兆帕)和Metaltite/Epricord(27.6±5.9兆帕)的最大剪切粘接强度最高,其次是Metaltite/PP、合金底漆、Metaltite、Metaltite/PM、金属底漆II、V-底漆和Epricord。PE、PM和PP的粘接强度最低。本研究结果表明,硫脲单体与磷酸盐单体的联合使用可改善粘接效果。据此,临床医生在制作树脂粘接假体时应注意底漆中溶解的功能性单体类型。