Jin E X, Xu X
School of Mechanical Engineering, Purdue University, West Lafayette, IN, USA.
J Microsc. 2008 Mar;229(Pt 3):503-11. doi: 10.1111/j.1365-2818.2008.01935.x.
Near-field optical probe is the key element of a near-field scanning optical microscopy (NSOM) system. The key innovation in the first two NSOM experiments (Pohl et al., 1984; Lewis et al., 1984) is the fabrications of a sub-wavelength optical aperture at the apex of a sharply pointed transparent probe tip with a thin metal coating. This paper discusses the routine use of focussed ion beam (FIB) to micro-machine NSOM aperture probes from the commercial silicon nitride cantilevered atomic force microscopy probes. Two FIB micro-machining approaches are used to form a nanoaperture of controllable size and shape at the apex of the tip. The FIB side slicing produces a silicon nitride aperture on the flat-end tips with controllable sizes varying from 120 nm to 30 nm. The FIB head-on drilling creates holes on the aluminium-coated tips with sizes down to 50 nm. Nanoapertures in C and bow tie shapes can also be patterned using the FIB head-on milling method to possibly enhance the optical transmission. A transmission-collection NSOM system is constructed from a commercial atomic force microscopy to characterize the optical resolution of FIB-micro-machined aperture tips. The optical resolution of 78 nm is demonstrated by an aperture probe fabricated by FIB head-on drilling. Simultaneous topography imaging can also be realized using the same probe. By mapping the optical near-field from a bow-tie aperture, optical resolution as small as 59 nm is achieved by an aperture probe fabricated by the FIB side slicing method. Overall, high resolution and reliable optical imaging of routinely FIB-micro-machined aperture probes are demonstrated.
近场光学探针是近场扫描光学显微镜(NSOM)系统的关键元件。前两个NSOM实验(Pohl等人,1984年;Lewis等人,1984年)的关键创新在于,在带有薄金属涂层的尖锐透明探针尖端的顶端制造出一个亚波长光学孔径。本文讨论了使用聚焦离子束(FIB)从商用氮化硅悬臂式原子力显微镜探针微加工NSOM孔径探针的常规方法。两种FIB微加工方法用于在探针尖端的顶端形成尺寸和形状可控的纳米孔径。FIB侧面切片在平头尖端上产生氮化硅孔径,其可控尺寸范围从120纳米到30纳米。FIB正面钻孔在涂铝尖端上钻出尺寸小至50纳米的孔。还可以使用FIB正面铣削方法对C形和领结形的纳米孔径进行图案化,以可能提高光传输。由商用原子力显微镜构建了一个透射-收集NSOM系统,以表征FIB微加工孔径尖端的光学分辨率。通过FIB正面钻孔制造的孔径探针展示了78纳米的光学分辨率。使用同一探针也可以实现同时形貌成像。通过绘制领结形孔径的光学近场,由FIB侧面切片方法制造的孔径探针实现了低至59纳米的光学分辨率。总体而言,展示了常规FIB微加工孔径探针的高分辨率和可靠光学成像。