Maurice C, Fortunier R
Ecole des Mines de Saint-Etienne, Centre SMS, UMR CNRS 5146, 158 cours Fauriel, 42023 Saint-Etienne Cedex 2, France.
J Microsc. 2008 Jun;230(Pt 3):520-9. doi: 10.1111/j.1365-2818.2008.02045.x.
A three-dimensional Hough transform is designed for the detection of conic curves (hyperbolae and ellipses) formed by the gnomonic projection of diffraction Kossel cones. This new procedure is applied to a high-angular-accuracy analysis of electron backscatter diffraction (EBSD) patterns and to a fully automatic indexing of X-ray Kossel patterns in the SEM. The high-accuracy analysis of EBSD patterns allows for the determination of local elastic strains, without any reference pattern, and with a spatial resolution of a few tens of nanometres. An accuracy of 2 x 10(-4) is achieved on geometrically calculated diagrams. This paper presents also the first fully automatic indexing of Kossel patterns. This automatic indexing procedure can be applied to local texture analysis, as well as to local elastic strain measurements. Although the spatial resolution of Kossel is about 1 microm, the accuracy of strain measurement is in this case much higher than that presently obtained on EBSD.
设计了一种三维霍夫变换,用于检测由衍射科塞尔锥的球心投影形成的圆锥曲线(双曲线和椭圆)。这一新方法应用于电子背散射衍射(EBSD)图案的高角度精度分析以及扫描电子显微镜(SEM)中X射线科塞尔图案的全自动索引。EBSD图案的高精度分析允许在无需任何参考图案的情况下确定局部弹性应变,空间分辨率可达几十纳米。在几何计算图上实现了2×10⁻⁴的精度。本文还介绍了科塞尔图案的首次全自动索引。这种自动索引程序可应用于局部织构分析以及局部弹性应变测量。尽管科塞尔的空间分辨率约为1微米,但在这种情况下应变测量的精度比目前在EBSD上获得的精度要高得多。