Incerti Matteo, Acquotti Domenico, Vicini Paola
Dipartimento Farmaceutico, Università degli Studi di Parma, Viale G. P. Usberti 27/A, Parma 43100, Italy.
Magn Reson Chem. 2008 Dec;46(12):1175-9. doi: 10.1002/mrc.2308.
The complete (1)H and (13)C NMR assignments of the novel compound methyl 2-amino-3-(benzo[d]isothiazol-3-yl)propanoate (1), of 3-amino-5-methylbenzo[d]isothiazole (2) and N-(t-butyloxycarbonyl)-2-aminobenzo[d]isothiazol-3(2H)-one (3) and of the desulfurated isostere of 3, N-(t-butyloxycarbonyl)-2-aminoisoindolin-1-one (4), using 1D and 2D NMR techniques, including COSY, INADEQUATE, HSQC, and HMBC experiments are reported.
报道了使用一维和二维核磁共振技术（包括COSY、INADEQUATE、HSQC和HMBC实验）对新型化合物2-氨基-3-（苯并[d]异噻唑-3-基）丙酸甲酯（1）、3-氨基-5-甲基苯并[d]异噻唑（2）、N-（叔丁氧基羰基）-2-氨基苯并[d]异噻唑-3（2H）-酮（3）以及3的脱硫类似物N-（叔丁氧基羰基）-2-氨基异吲哚啉-1-酮（4）的完整氢谱和碳谱归属。
