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The iodometric determination of dithionite, thiosulphate and sulphite in the presence of alkali and/or cyanide.

作者信息

Kilroy W P

机构信息

Naval Surface Weapons Center, White Oak Laboratory, Silver Spring, Maryland 20910, U.S.A.

出版信息

Talanta. 1980 Apr;27(4):343-7. doi: 10.1016/0039-9140(80)80093-2.

Abstract

The analysis of mixtures of dithionite, thiosulphate and sulphite in the presence of cyanide and/or in alkaline solution has been investigated. The effects of such constituents as sulphur, acetonitrile, hexafluoroarsenate, and bromide in alkaline solution were also examined. Satisfactory results were obtained by using low-temperature, oxygen-free, alkaline solutions, containing excess of alkali, at pH > 12.

摘要

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