Dills R L, Kent S D, Checkoway H, Kalman D A
Department of Environmental Health, School of Public Health and Community Medicine, University of Washington, Seattle, WA 98195, U.S.A.
Talanta. 1991 Apr;38(4):365-74. doi: 10.1016/0039-9140(91)80073-9.
A static headspace method for determination of volatile solvents in blood was developed. The solvents determined were 1,1,1-trichloroethane, toluene, xylene (o-, m- and p-), ethylbenzene, styrene, alpha-methylstyrene and 4-methylstyrene at concentrations ranging from 0.01 to 1 mug/ml. Internal standard calibration was used. Parameters affecting sensitivity and precision were determined and optimized.
建立了一种用于测定血液中挥发性溶剂的静态顶空法。所测定的溶剂为1,1,1-三氯乙烷、甲苯、二甲苯（邻、间和对）、乙苯、苯乙烯、α-甲基苯乙烯和4-甲基苯乙烯，浓度范围为0.01至1微克/毫升。采用内标校准。确定并优化了影响灵敏度和精密度的参数。
