Imbaud Joël, Boy Jean-Jacques, Galliou Serge, Bourquin Roger, Romand Jean Pierre
Laboratoire de Chronometrie d'Electronique et de Piezoelectricite Department, Franche Comte Electronique Mecanique Thermique et Optique-Sciences et Technologies Institute, Besancon, France.
IEEE Trans Ultrason Ferroelectr Freq Control. 2008 Nov;55(11):2384-91. doi: 10.1109/TUFFC.946.
The LGS family are promising materials for the design of high quality bulk acoustic wave resonators. We have manufactured many plano-convex 10 MHz 5th overtone Y-cut resonators using langasite (LGS, La(3)Ga(5)SiO(14)) and langatate (LGT, La(3)Ga(5.5)Ta(0.5)O(14)) crystals. We observed that the quality factor strongly depends on the polishing method, the supplier of the material, and on the energy trapping. For quartz crystals, we have found that resulting IR spectra exhibit absorption peaks more or less deep, linked to defects. These predominant criteria are not surprising, but they have to be defined in manner similar to that used for quartz crystal. A satisfying machining and polishing method has been first applied to elaborate high Q resonators, and a comparison between samples of LGS and LGT materials from different suppliers is established. In addition, LGT resonators are characterized by their motional parameters and frequency-temperature curves. Nevertheless, one of the main results is that the measured Q x f product is not the expected one. We present results of Q-factor versus radius of curvature: it appears that an optimization should be performed and that this last one cannot be directly transposed from that of quartz crystal resonator. Currently, the best resonator that we have made has a Q x f product of 1.4 x 10(13) on its 5th overtone (1.7 x 10(13) on its 9th overtone). This result is slightly higher than the similar parameter obtained on a state-of-the-art SC-cut quartz crystal resonator working at the same frequency.
LGS族是用于设计高质量体声波谐振器的有前途的材料。我们使用硅酸镧镓(LGS,La(3)Ga(5)SiO(14))和镓酸镧钽(LGT,La(3)Ga(5.5)Ta(0.5)O(14))晶体制造了许多平凸10MHz第五泛音Y切谐振器。我们观察到品质因数强烈依赖于抛光方法、材料供应商以及能量俘获。对于石英晶体,我们发现所得的红外光谱或多或少会出现与缺陷相关的深浅不同的吸收峰。这些主要标准并不令人惊讶,但必须以类似于用于石英晶体的方式来定义。首先应用了一种令人满意的加工和抛光方法来制造高Q值谐振器,并对来自不同供应商的LGS和LGT材料样品进行了比较。此外,LGT谐振器通过其运动参数和频率-温度曲线来表征。然而,主要结果之一是测得的Q×f乘积并非预期值。我们给出了品质因数与曲率半径的关系结果:似乎应该进行优化,并且不能直接将石英晶体谐振器的优化方法照搬过来。目前,我们制造的最佳谐振器在其第五泛音时的Q×f乘积为1.4×10(13)(在其第九泛音时为1.7×10(13))。这个结果略高于在相同频率下工作的最先进的SC切石英晶体谐振器所获得的类似参数。