Wu Sean, Yan Guo-Jun, Lee Maw-Shung, Ro Ruyen, Chen K I
Department of Electronics Engineering and Computer Science, Tung Fang Institute of Technology, Hunei Shiang, Kaohsiung County, Taiwan, R.O.C.
IEEE Trans Ultrason Ferroelectr Freq Control. 2007 Dec;54(12):2456-61. doi: 10.1109/TUFFC.2007.559.
C-axis-oriented ZnO films were sputtered on Langasite substrate (LGS, La(3)Ga(5)SiO(14)). The crystalline structure of the films was determined by grazing incident angle X-ray diffraction, the surface microstructure of films was investigated by scanning electron microscopy and atomic force microscopy, the atom composition ratio O/Zn of films was determined by energy dispersive X-ray spectroscopy, and the resistivity of films was determined by the four-point probe instrument. The measurement results showed those films prepared were all polycrystalline hexagonal ZnO films. By analyzing the microstructure of the ZnO films, those prepared at the oxygen flow rate (O(2)/O(2)+Ar) of 20%, the RF power of 200 W, and the substrate temperature of 200 degrees C had the best performance: highly c-axis-oriented microstructures, dense surface morphology, and the atom composition ratio 1.02. The measured scattering parameters of the SAW device fabricated on the composite substrate (ZnO/LGS) with film thickness 1.76 microm showed an average shifted velocity around 2741 m/s at 57.1 MHz and a electromagnetic coupling coefficient greater than 1%.
在硅酸镧镓(LGS,La(3)Ga(5)SiO(14))衬底上溅射制备了C轴取向的氧化锌薄膜。通过掠入射角X射线衍射确定薄膜的晶体结构,利用扫描电子显微镜和原子力显微镜研究薄膜的表面微观结构,通过能量色散X射线光谱法测定薄膜的原子组成比O/Zn,并用四点探针仪测定薄膜的电阻率。测量结果表明,所制备的薄膜均为多晶六方氧化锌薄膜。通过分析氧化锌薄膜的微观结构,发现在氧气流量(O(2)/O(2)+Ar)为20%、射频功率为200W、衬底温度为200℃条件下制备的薄膜性能最佳:具有高度C轴取向的微观结构、致密的表面形貌以及原子组成比为1.02。在厚度为1.76μm的复合衬底(ZnO/LGS)上制备的声表面波器件的测量散射参数显示,在57.1MHz时平均偏移速度约为2741m/s,电磁耦合系数大于1%。