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复合树脂在酸性药物和pH循环作用下的表面降解

Surface degradation of composite resins by acidic medicines and pH-cycling.

作者信息

Valinoti Ana Carolina, Neves Beatriz Gonçalves, da Silva Eduardo Moreira, Maia Lucianne Cople

机构信息

Department of Pediatric Dentistry and Orthodontics, Dental School, Federal University of Rio de Janeiro, Rio de Janeiro, RJ, Brazil.

出版信息

J Appl Oral Sci. 2008 Jul-Aug;16(4):257-65. doi: 10.1590/s1678-77572008000400006.

Abstract

This study evaluated the effects of acidic medicines (Dimetapp and Claritin), under pH-cycling conditions, on the surface degradation of four composite resins (microhybrid: TPH, Concept, Opallis and Nanofilled: Supreme). Thirty disc-shaped specimens ([symbol: see text] = 5.0 mm/thickness = 2.0 mm) of each composite were randomly assigned to 3 groups (n = 10): a control and two experimental groups, according to the acidic medicines evaluated. The specimens were finished and polished with aluminum oxide discs, and the surface roughness was measured by using a profilometer. After the specimens were submitted to a pH-cycling regimen and immersion in acidic medicines for 12 days, the surface roughness was measured again. Two specimens for each material and group were analyzed by scanning electron microscopy (SEM) before and after pH-cycling. Data were analyzed by the Student's-t test, ANOVA, Duncan's multiple range test and paired t-test (alpha=0.05). Significant increase in roughness was found only for TPH in the control group and TPH and Supreme immersed in Claritin (p<0.05). SEM analyses showed that the 4 composite resins underwent erosion and surface degradation after being subjected to the experimental conditions. In conclusion, although the roughness was slightly affected, the pH-cycling and acidic medicines caused surface degradation of the composite resins evaluated. Titratable acidity seemed to play a more crucial role on surface degradation of composite resins than pH.

摘要

本研究评估了在pH循环条件下,酸性药物(迪美泰和平奇)对四种复合树脂(微混合树脂:TPH、Concept、Opallis和纳米填充树脂:Supreme)表面降解的影响。每种复合树脂制备30个圆盘形试件(直径 = 5.0 mm/厚度 = 2.0 mm),根据所评估的酸性药物随机分为3组(n = 10):一组为对照组,两组为实验组。试件用氧化铝圆盘进行修整和抛光,并用轮廓仪测量表面粗糙度。在试件接受pH循环方案并浸泡在酸性药物中12天后,再次测量表面粗糙度。在pH循环前后,每组每种材料取两个试件通过扫描电子显微镜(SEM)进行分析。数据采用Student's-t检验、方差分析、邓肯多重极差检验和配对t检验进行分析(α = 0.05)。仅发现对照组中的TPH以及浸泡在平奇中的TPH和Supreme的粗糙度有显著增加(p<0.05)。SEM分析表明,4种复合树脂在经受实验条件后均发生了侵蚀和表面降解。总之,尽管粗糙度受到的影响较小,但pH循环和酸性药物导致了所评估复合树脂的表面降解。可滴定酸度似乎比pH对复合树脂的表面降解起着更关键的作用。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/3238/4327534/30447ebd38a4/1678-7757-jaos-16-04-0257-gf01.jpg

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