Ishikiriama Sérgio Kiyoshi, De Oliveira Gabriela Ulian, Maenosono Rafael Massunari, Wang Linda, Duarte Marco Antonio Húngaro, Mondelli Rafael Francisco Lia
Am J Dent. 2014 Aug;27(4):195-8.
To evaluate the effects of toothbrushing abrasion associated with pH cycling on the surface roughness and wear of methacrylate- and silorane-based resin composites.
Microhybrid methacrylate-based (Filtek Z250), nanofilled methacrylate-based (Filtek Supreme Ultra) and microhybrid silorane-based (Filtek LS) composites were selected for this investigation. For each composite, two groups (n = 10) of rectangular specimens were made. The initial roughness (Ra) of all of the groups was evaluated based on the average of three random tracings with a profilometer, and each specimen had half of its surface protected with two layers of nail varnish to serve as controls. Half of the specimens of each resin were submitted to pH cycling, while the other half were stored in deionized water for 14 days. Subsequently, 100,000 strokes of simulated toothbrushing were performed. Final roughness and wear were measured with the same profilometer, and the values were submitted to ANOVA, Student's t-test and Tukey's test (P < 0.05).
The data revealed an increase in surface roughness for Filtek Z250 and Filtek Supreme Ultra after toothbrushing, while Filtek LS showed the opposite behavior. Methacrylate-based composites presented lower wear values [Z250 (4.19 ± 1.73 μm); Supreme Ultra (4.16 ± 0.95 μm)], while the silorane-based composite presented increased surface roughness (11.51 ± 5.69 μm), particularly when submitted to pH cycling (15.31 ± 5.41 μm). Despite the good properties of silorane-based composites, particularly its smooth surface roughness even after pH cycling and toothbrushing abrasion, this composite still presented increased wear, which is an important issue for the development of new resin compositions.
评估与pH循环相关的刷牙磨损对甲基丙烯酸酯基和硅氧烷基树脂复合材料表面粗糙度和磨损的影响。
本研究选用了基于微混合甲基丙烯酸酯的(Filtek Z250)、纳米填充甲基丙烯酸酯的(Filtek Supreme Ultra)和基于微混合硅氧烷的(Filtek LS)复合材料。对于每种复合材料,制作两组(n = 10)矩形试件。基于用轮廓仪进行的三次随机描记的平均值评估所有组的初始粗糙度(Ra),并且每个试件的一半表面用两层指甲油保护作为对照。每种树脂的一半试件进行pH循环,而另一半在去离子水中储存14天。随后,进行100,000次模拟刷牙冲程。用同一轮廓仪测量最终粗糙度和磨损,并将这些值进行方差分析、学生t检验和Tukey检验(P < 0.05)。
数据显示,刷牙后Filtek Z250和Filtek Supreme Ultra的表面粗糙度增加,而Filtek LS表现出相反的情况。基于甲基丙烯酸酯的复合材料呈现较低的磨损值[Z250(4.19±1.73μm);Supreme Ultra(4.16±0.95μm)],而基于硅氧烷的复合材料表面粗糙度增加(11.51±5.69μm),特别是在进行pH循环时(15.31±5.4μm)。尽管基于硅氧烷的复合材料具有良好的性能,特别是即使在pH循环和刷牙磨损后其表面粗糙度仍很光滑,但这种复合材料仍呈现出磨损增加的情况,这对于新型树脂组合物的开发来说是一个重要问题。