Amm Elie W, Hardan Louis S, BouSerhal Joseph P, Glasl Bettina, Ludwig Björn
Department of Orthodontics, School of Dental Medicine, Saint Joseph University, Beirut, Lebanon.
J Orofac Orthop. 2008 Sep;69(5):383-92. doi: 10.1007/s00056-008-0812-8.
The purpose of this study was to evaluate the shear bond strength of orthodontic bracket when bonded to pre-conditioned and intact enamel using a self-etching primer within 6 hours and after thermal cycling.
One hundred and twenty freshly-extracted human teeth were divided into four groups according to how the buccal surface to be bonded had been pre-conditioned: 1) acid-etched with 37% phosphoric acid, 2) sand-blasted with 50 microns aluminum-oxide, 3) matted with diamond burr, and 4) intact enamel used as control. Orthodontic metal brackets were bonded to the teeth using the same composite resin (Transbond XT) and self-etching primer (Transbond Plus Self-Etching Primer). Brackets were debonded within 6 hours or after thermal cycling for 2500 times (5 degrees C--37 degrees C--55 degrees C). Shear bond strength was measured on a testing machine at a crosshead speed of 3 mm/min. The bracket-failure interface was quantified according to the modified adhesive remnant index score (ARI). Data were analyzed using the two-way ANOVA test, Scheffé confidence interval of differences of means, and the chi-square test (p < 0.05).
All the pre-conditioned groups showed significantly higher shear bond strength before and after thermal cycling than the control group. There was no significant correlation between thermal cycling and shear bond strength. The ARI scores revealed that the bond failed primarily on the adhesive-enamel interface in all groups before and after thermal cycling, with the exception of the acid-etched group, whose bonds failed mainly on the adhesive-bracket interface after thermal cycling.
The authors recommend that the enamel be preconditioned before applying the self-etching primer when greater shear bond strength is desired.
本研究旨在评估正畸托槽在使用自酸蚀底漆粘结到预处理和完整釉质上6小时后以及热循环后的剪切粘结强度。
120颗新鲜拔除的人牙根据待粘结颊面的预处理方式分为四组:1)用37%磷酸酸蚀;2)用50微米氧化铝喷砂;3)用金刚石车针打磨;4)完整釉质作为对照组。使用相同的复合树脂(Transbond XT)和自酸蚀底漆(Transbond Plus自酸蚀底漆)将正畸金属托槽粘结到牙齿上。托槽在6小时内或热循环2500次(5℃-37℃-55℃)后脱粘。在测试机上以3毫米/分钟的十字头速度测量剪切粘结强度。根据改良的粘结剂残留指数评分(ARI)对托槽-失败界面进行量化。使用双向方差分析测试、均值差异的Scheffé置信区间和卡方检验(p<0.05)对数据进行分析。
所有预处理组在热循环前后的剪切粘结强度均显著高于对照组。热循环与剪切粘结强度之间无显著相关性。ARI评分显示,除酸蚀组外,所有组在热循环前后粘结主要在粘结剂-釉质界面失败,酸蚀组在热循环后粘结主要在粘结剂-托槽界面失败。
作者建议,当需要更高的剪切粘结强度时,在应用自酸蚀底漆之前应对釉质进行预处理。