Sarin P, Haggerty R P, Yoon W, Knapp M, Berghaeuser A, Zschack P, Karapetrova E, Yang N, Kriven W M
Department of Materials Science and Engineering, University of Illinois at Urbana-Champaign, IL 61801, USA.
J Synchrotron Radiat. 2009 Mar;16(Pt 2):273-82. doi: 10.1107/S0909049509001265. Epub 2009 Feb 3.
The developed curved image plate (CIP) is a one-dimensional detector which simultaneously records high-resolution X-ray diffraction (XRD) patterns over a 38.7 degrees 2theta range. In addition, an on-site reader enables rapid extraction, transfer and storage of X-ray intensity information in </=30 s, and further qualifies this detector to study kinetic processes in materials science. The CIP detector can detect and store X-ray intensity information linearly proportional to the incident photon flux over a dynamical range of about five orders of magnitude. The linearity and uniformity of the CIP detector response is not compromised in the unsaturated regions of the image plate, regardless of saturation in another region. The speed of XRD data acquisition together with excellent resolution afforded by the CIP detector is unique and opens up wide possibilities in materials research accessible through X-ray diffraction. This article presents details of the basic features, operation and performance of the CIP detector along with some examples of applications, including high-temperature XRD.
所开发的弯曲成像板(CIP)是一种一维探测器,可在38.7度2θ范围内同时记录高分辨率X射线衍射(XRD)图案。此外,现场读取器能够在≤30秒内快速提取、传输和存储X射线强度信息,这进一步使该探测器有资格用于研究材料科学中的动力学过程。CIP探测器能够在约五个数量级的动态范围内检测和存储与入射光子通量成线性比例的X射线强度信息。在成像板的不饱和区域,CIP探测器响应的线性度和均匀性不受影响,无论其他区域是否饱和。CIP探测器提供的XRD数据采集速度以及出色的分辨率是独一无二的,为通过X射线衍射进行材料研究开辟了广泛的可能性。本文介绍了CIP探测器的基本特征、操作和性能细节以及一些应用示例,包括高温XRD。