• 文献检索
  • 文档翻译
  • 深度研究
  • 学术资讯
  • Suppr Zotero 插件Zotero 插件
  • 邀请有礼
  • 套餐&价格
  • 历史记录
应用&插件
Suppr Zotero 插件Zotero 插件浏览器插件Mac 客户端Windows 客户端微信小程序
定价
高级版会员购买积分包购买API积分包
服务
文献检索文档翻译深度研究API 文档MCP 服务
关于我们
关于 Suppr公司介绍联系我们用户协议隐私条款
关注我们

Suppr 超能文献

核心技术专利：CN118964589B侵权必究
粤ICP备2023148730 号-1Suppr @ 2026

文献检索

告别复杂PubMed语法，用中文像聊天一样搜索，搜遍4000万医学文献。AI智能推荐，让科研检索更轻松。

立即免费搜索

文件翻译

保留排版，准确专业，支持PDF/Word/PPT等文件格式，支持 12+语言互译。

免费翻译文档

深度研究

AI帮你快速写综述，25分钟生成高质量综述，智能提取关键信息，辅助科研写作。

立即免费体验

瑞士光源 X 射线粉末衍射实验用 MYTHEN 探测器。

The MYTHEN detector for X-ray powder diffraction experiments at the Swiss Light Source.

机构信息

Paul Scherrer Institut, CH-5232 Villigen, Switzerland.

出版信息

J Synchrotron Radiat. 2010 Sep;17(5):653-68. doi: 10.1107/S0909049510026051. Epub 2010 Jul 22.

DOI:10.1107/S0909049510026051
PMID:20724787
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC2924792/
Abstract

The MYTHEN single-photon-counting silicon microstrip detector has been developed at the Swiss Light Source for time-resolved powder diffraction experiments. An upgraded version of the detector has been installed at the SLS powder diffraction station allowing the acquisition of diffraction patterns over 120 degrees in 2theta in fractions of seconds. Thanks to the outstanding performance of the detector and to the calibration procedures developed, the quality of the data obtained is now comparable with that of traditional high-resolution point detectors in terms of FWHM resolution and peak profile shape, with the additional advantage of fast and simultaneous acquisition of the full diffraction pattern. MYTHEN is therefore optimal for time-resolved or dose-critical measurements. The characteristics of the MYTHEN detector together with the calibration procedures implemented for the optimization of the data are described in detail. The refinements of two known standard powders are discussed together with a remarkable application of MYTHEN to organic compounds in relation to the problem of radiation damage.

摘要

瑞士光源开发了用于时间分辨粉末衍射实验的 MYTHEN 单光子计数硅微条探测器。探测器的升级版本已安装在 SLS 粉末衍射站，允许在 2θ 上采集超过 120 度的衍射图案，时间为几分之一秒。由于探测器的出色性能和开发的校准程序，与传统的高分辨率点探测器相比，现在获得的数据质量在 FWHM 分辨率和峰形方面具有可比性，并且具有快速同时采集完整衍射图案的额外优势。因此，MYTHEN 非常适合时间分辨或剂量关键测量。详细描述了 MYTHEN 探测器的特性以及为优化数据而实施的校准程序。讨论了两个已知标准粉末的改进，以及 MYTHEN 在与辐射损伤问题相关的有机化合物方面的一个显著应用。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2431/2924792/845fac372744/s-17-00653-fig15.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2431/2924792/bb6ba624eb74/s-17-00653-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2431/2924792/215c3c62e4df/s-17-00653-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2431/2924792/cfa3e8f967c1/s-17-00653-fig3.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2431/2924792/e52f051d2519/s-17-00653-fig4.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2431/2924792/45379e13481c/s-17-00653-fig5.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2431/2924792/94875aade154/s-17-00653-fig6.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2431/2924792/47ab9415ca63/s-17-00653-fig7.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2431/2924792/8d6df2419698/s-17-00653-fig8.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2431/2924792/9023445e531e/s-17-00653-fig9.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2431/2924792/e5d77063df55/s-17-00653-fig10.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2431/2924792/a7ddc21a8c22/s-17-00653-fig11.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2431/2924792/ea43eab12f1f/s-17-00653-fig12.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2431/2924792/8505d39f7315/s-17-00653-fig13.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2431/2924792/57566ff6503a/s-17-00653-fig14.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2431/2924792/845fac372744/s-17-00653-fig15.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2431/2924792/bb6ba624eb74/s-17-00653-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2431/2924792/215c3c62e4df/s-17-00653-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2431/2924792/cfa3e8f967c1/s-17-00653-fig3.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2431/2924792/e52f051d2519/s-17-00653-fig4.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2431/2924792/45379e13481c/s-17-00653-fig5.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2431/2924792/94875aade154/s-17-00653-fig6.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2431/2924792/47ab9415ca63/s-17-00653-fig7.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2431/2924792/8d6df2419698/s-17-00653-fig8.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2431/2924792/9023445e531e/s-17-00653-fig9.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2431/2924792/e5d77063df55/s-17-00653-fig10.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2431/2924792/a7ddc21a8c22/s-17-00653-fig11.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2431/2924792/ea43eab12f1f/s-17-00653-fig12.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2431/2924792/8505d39f7315/s-17-00653-fig13.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2431/2924792/57566ff6503a/s-17-00653-fig14.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2431/2924792/845fac372744/s-17-00653-fig15.jpg

相似文献

1
The MYTHEN detector for X-ray powder diffraction experiments at the Swiss Light Source.瑞士光源 X 射线粉末衍射实验用 MYTHEN 探测器。
J Synchrotron Radiat. 2010 Sep;17(5):653-68. doi: 10.1107/S0909049510026051. Epub 2010 Jul 22.
2
A twelve-analyzer detector system for high-resolution powder diffraction.用于高分辨率粉末衍射的十二分析仪探测器系统。
J Synchrotron Radiat. 2008 Sep;15(Pt 5):427-32. doi: 10.1107/S0909049508018438. Epub 2008 Jul 22.
3
X-ray powder diffraction beamline at D10B of LNLS: application to the Ba2FeReO6 double perovskite.巴西国家同步辐射实验室D10B的X射线粉末衍射光束线：在Ba2FeReO6双钙钛矿中的应用
J Synchrotron Radiat. 2006 Jan;13(Pt 1):46-53. doi: 10.1107/S0909049505039208. Epub 2005 Dec 22.
4
Multipole electron densities and structural parameters from synchrotron powder X-ray diffraction data obtained with a MYTHEN detector system (OHGI).使用MYTHEN探测器系统（OHGI）获得的同步辐射粉末X射线衍射数据的多极电子密度和结构参数。
Acta Crystallogr A Found Adv. 2021 Mar 1;77(Pt 2):85-95. doi: 10.1107/S2053273320016605. Epub 2021 Jan 28.
5
Applications of Powder X-Ray Diffraction in Small Molecule Pharmaceuticals: Achievements and Aspirations.粉末 X 射线衍射在小分子药物中的应用：成就与展望。
J Pharm Sci. 2018 Dec;107(12):2969-2982. doi: 10.1016/j.xphs.2018.08.010. Epub 2018 Aug 23.
6
High-resolution and high-intensity powder diffractometer at BL15XU in SPring-8.位于日本理化学研究所八重洲实验室15号光束线（BL15XU）的高分辨率高强度粉末衍射仪。
J Synchrotron Radiat. 2003 Nov 1;10(Pt 6):424-9. doi: 10.1107/s0909049503018296. Epub 2003 Oct 10.
7
Application of a hybrid pixel detector to powder diffraction.混合像素探测器在粉末衍射中的应用。
J Synchrotron Radiat. 2007 Jan;14(Pt 1):151-7. doi: 10.1107/S0909049506048783. Epub 2006 Dec 15.
8
New perspectives in macromolecular powder diffraction using single-photon-counting strip detectors: high-resolution structure of the pharmaceutical peptide octreotide.使用单光子计数条探测器研究大分子粉末衍射的新视角：药物肽奥曲肽的高分辨率结构。
Acta Crystallogr A Found Adv. 2021 May 1;77(Pt 3):186-195. doi: 10.1107/S2053273321001698. Epub 2021 Mar 12.
9
Combinatorial screening employing nylon loops and micro-X-ray powder diffraction.采用尼龙环和微X射线粉末衍射的组合筛选
J Pharm Biomed Anal. 2005 Mar 9;37(3):611-4. doi: 10.1016/j.jpba.2004.11.007. Epub 2004 Dec 15.
10
Combined synchrotron X-ray tomography and X-ray powder diffraction using a fluorescing metal foil.结合使用荧光金属箔的同步加速器X射线断层扫描和X射线粉末衍射。
Rev Sci Instrum. 2013 Jun;84(6):063703. doi: 10.1063/1.4810011.

引用本文的文献

1
MYTHEN III: advancements in single photon counting detectors for synchrotron powder diffraction experiments.MYTHEN III：用于同步辐射粉末衍射实验的单光子计数探测器的进展
J Synchrotron Radiat. 2025 Mar 1;32(Pt 2):365-377. doi: 10.1107/S1600577525000438. Epub 2025 Feb 13.
2
High-throughput and high-resolution powder X-ray diffractometer consisting of six sets of 2D CdTe detectors with variable sample-to-detector distance and innovative automation system.高通量高分辨率粉末X射线衍射仪，由六组二维碲化镉探测器组成，探测器与样品距离可变，并配备创新自动化系统。
J Synchrotron Radiat. 2024 Jul 1;31(Pt 4):955-967. doi: 10.1107/S1600577524003539. Epub 2024 Jun 20.
3

本文引用的文献

1
The High Resolution Powder Diffraction Beam Line at ESRF.欧洲同步辐射装置的高分辨率粉末衍射光束线。
J Res Natl Inst Stand Technol. 2004 Feb 1;109(1):133-142. doi: 10.6028/jres.109.010. Print 2004 Jan-Feb.
2
Molecular and crystalline structures of three (S)-4-alkoxycarbonyl-2-azetidinones containing long alkyl side chains from synchrotron X-ray powder diffraction data.
Acta Crystallogr B. 2009 Dec;65(Pt 6):724-30. doi: 10.1107/S0108768109036386. Epub 2009 Nov 16.
3
X-ray pair distribution function analysis of nanostructured materials using a Mythen detector.使用 Myhten 探测器对纳米结构材料的 X 射线对分布函数进行分析。
Coupling to octahedral tilts in halide perovskite nanocrystals induces phonon-mediated attractive interactions between excitons.
与卤化物钙钛矿纳米晶体中的八面体倾斜耦合会诱导激子之间由声子介导的吸引相互作用。
Nat Phys. 2024;20(1):47-53. doi: 10.1038/s41567-023-02253-7. Epub 2023 Nov 9.
4
Exploring high-throughput synchrotron X-Ray powder diffraction for the structural analysis of pharmaceuticals.探索高通量同步加速器X射线粉末衍射用于药物的结构分析。
Int J Pharm X. 2023 Nov 29;6:100221. doi: 10.1016/j.ijpx.2023.100221. eCollection 2023 Dec 15.
5
Structural insight into the cooperativity of spin crossover compounds.自旋交叉化合物协同性的结构洞察。
Acta Crystallogr B Struct Sci Cryst Eng Mater. 2023 Oct 1;79(Pt 5):354-367. doi: 10.1107/S2052520623005814. Epub 2023 Aug 11.
6
Energy Transfer from Magnetic Iron Oxide Nanoparticles: Implications for Magnetic Hyperthermia.磁性氧化铁纳米颗粒的能量转移：对磁热疗的影响。
ACS Appl Nano Mater. 2023 May 17;6(14):12914-12921. doi: 10.1021/acsanm.3c01643. eCollection 2023 Jul 28.
7
Total scattering measurements at the Australian Synchrotron Powder Diffraction beamline: capabilities and limitations.在澳大利亚同步加速器粉末衍射光束线上进行总散射测量：能力和限制。
J Synchrotron Radiat. 2023 Mar 1;30(Pt 2):327-339. doi: 10.1107/S1600577522011614. Epub 2023 Jan 13.
8
Strongly Confined CsPbBr Quantum Dots as Quantum Emitters and Building Blocks for Rhombic Superlattices.强受限 CsPbBr 量子点作为量子发射器和菱形超晶格的构建块。
ACS Nano. 2023 Feb 14;17(3):2089-2100. doi: 10.1021/acsnano.2c07677. Epub 2023 Jan 31.
9
A compact-rigid multi-analyser for energy and angle filtering of high-resolution X-ray experiments. Part 2. Efficiency of a single-crystal-comb.紧凑型刚性多分析器，用于对高分辨率 X 射线实验进行能量和角度滤波。第 2 部分。单晶梳的效率。
J Synchrotron Radiat. 2023 Jan 1;30(Pt 1):126-136. doi: 10.1107/S1600577522011250.
10
A compact-rigid multi-analyser for energy and angle filtering of high-resolution X-ray experiments. Part 1. Principles and implementation.一种紧凑刚性的多分析器，用于对高分辨率 X 射线实验进行能量和角度滤波。第 1 部分：原理与实现。
J Synchrotron Radiat. 2023 Jan 1;30(Pt 1):111-125. doi: 10.1107/S160057752201116X.
J Synchrotron Radiat. 2009 Nov;16(Pt 6):849-56. doi: 10.1107/S0909049509036723. Epub 2009 Sep 29.
4
Synchrotron radiation hardness studies of PILATUS II.PILATUS II的同步辐射硬度研究。
J Synchrotron Radiat. 2009 Jul;16(Pt 4):489-93. doi: 10.1107/S0909049509014733. Epub 2009 May 14.
5
Performance of single-photon-counting PILATUS detector modules.单光子计数型PILATUS探测器模块的性能
J Synchrotron Radiat. 2009 May;16(Pt 3):368-75. doi: 10.1107/S0909049509009911. Epub 2009 Apr 7.
6
Correcting electron-density resolution bias in reciprocal space.校正倒易空间中的电子密度分辨率偏差。
Acta Crystallogr A. 2009 May;65(Pt 3):183-9. doi: 10.1107/S0108767309003687. Epub 2009 Mar 13.
7
A curved image-plate detector system for high-resolution synchrotron X-ray diffraction.一种用于高分辨率同步加速器X射线衍射的弯曲成像板探测器系统。
J Synchrotron Radiat. 2009 Mar;16(Pt 2):273-82. doi: 10.1107/S0909049509001265. Epub 2009 Feb 3.
8
Characterization of four crystal polymorphs and a monohydrate of s-bupivacaine hydrochloride (levobupivacaine hydrochloride).盐酸左旋布比卡因（左旋布比卡因盐酸盐）的四种晶体多晶型物和一种一水合物的表征
J Pharm Sci. 2009 Mar;98(3):1064-74. doi: 10.1002/jps.21496.
9
Synchrotron applications of an amorphous silicon flat-panel detector.非晶硅平板探测器的同步加速器应用。
J Synchrotron Radiat. 2008 Sep;15(Pt 5):477-88. doi: 10.1107/S090904950801755X. Epub 2008 Jul 11.
10
A twelve-analyzer detector system for high-resolution powder diffraction.用于高分辨率粉末衍射的十二分析仪探测器系统。
J Synchrotron Radiat. 2008 Sep;15(Pt 5):427-32. doi: 10.1107/S0909049508018438. Epub 2008 Jul 22.