Nakamura E, Kuwajima I, Williard P G
Department of Chemistry, Tokyo Institute of Technology, Japan.
Acta Crystallogr C. 1991 May 15;47 ( Pt 5):984-5. doi: 10.1107/s010827019000909x.
Mr = 281.30, monoclinic, P2(1)/n, a = 10.966 (4), b = 7.170 (3), c = 15.976 (4) A, beta = 93.14 (2) degrees, V = 1254.3 (9) A3, Z = 4, Dx = 1.16 g cm-3, lambda (Mo K alpha) = 0.71069 A, mu = 0.706 cm-1, F(000) = 472, T = 295 K, final R = 0.057 for 1212 unique observed reflections. The compound was prepared by reaction of the trichlorotitanium-delta 1(2)-enolate of 2-methylcyclohexanone with benzaldehyde.
Mr = 281.30，单斜晶系，P2(1)/n，a = 10.966 (4)，b = 7.170 (3)，c = 15.976 (4) Å，β = 93.14 (2)°，V = 1254.3 (9) ų，Z = 4，Dx = 1.16 g cm⁻³，λ(Mo Kα) = 0.71069 Å，μ = 0.706 cm⁻¹，F(000) = 472，T = 295 K，对于1212个独特的观测反射，最终R = 0.057。该化合物是通过2-甲基环己酮的三氯钛-δ¹(2)-烯醇盐与苯甲醛反应制备的。
