Klein C L, Banks T A, Rouselle D
Department of Chemistry, Xavier University of Louisiana, New Orleans 70125.
Acta Crystallogr C. 1991 Jul 15;47 ( Pt 7):1478-80. doi: 10.1107/s010827019001280x.
C19H22N+.Cl-, Mr = 299.84, monoclinic, P2(1)/c, a = 5.070 (2), b = 34.088 (5), c = 9.976 (1) A, beta = 90.74 (2) degrees, V = 1724.0 A3, Z = 4, Dx = 1.16 g cm-3, lambda (Mo K alpha 1) = 0.70930 A, mu = 2.2 cm-1, F(000) = 640, T = 295 K, final R = 0.046 for 1381 observed reflections. The nortriptyline molecule crystallized with a 'butterfly' fold angle of 124.3 (2) degrees and an extended propylamino side chain. The amino nitrogen is involved in hydrogen bonds to two different chloride ions.
C19H22N⁺·Cl⁻，Mr = 299.84，单斜晶系，P2(1)/c，a = 5.070(2)，b = 34.088(5)，c = 9.976(1) Å，β = 90.74(2)°，V = 1724.0 ų，Z = 4，Dx = 1.16 g cm⁻³，λ(Mo Kα1) = 0.70930 Å，μ = 2.2 cm⁻¹，F(000) = 640，T = 295 K，对于1381个观测反射，最终R = 0.046。去甲替林分子以124.3(2)°的“蝴蝶”折叠角和一个伸展的丙氨基侧链结晶。氨基氮参与与两个不同氯离子的氢键形成。
